Dynamic recrystallization characteristics and processing map development of Mn-Ni-Mo steel using constitutive modeling

IF 7 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Science and Engineering: A Pub Date : 2025-02-01 DOI:10.1016/j.msea.2024.147672
Rahul Ranjan, Anil Meena
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Abstract

The manufacturing of reactor pressure vessels (RPVs) involves a complex multi-stage forging process with varying strain, temperature, and strain rate, resulting in dynamic recrystallization (DRX), dynamic recovery, and work hardening. These processes continuously alter the steel's microstructure, making it challenging to predict its final properties. This study addresses this challenge by investigating the hot deformation characteristics of Mn-Ni-Mo steel through compression tests using the Gleeble 3500 simulator. Tests were performed across temperatures from 900 °C 1200 °C and strain rates from 0.001 s−1 1 s−1. The effects of temperature, strain rate, and strain on DRX were investigated by examining work hardening rate flow stress curves and microstructural evolution. A hyperbolic sine constitutive equation was employed to model the relationship between peak stress, strain rate, and deformation temperature. Results revealed that higher deformation temperatures or lower strain rates reduce the critical strain for DRX and increase the DRX volume fraction. The strain rate sensitivity (SRS) of the steel varies with strain and temperature, with significant variations at lower strain rates (0.001 s−1 and 0.01 s−1) but decreasing at higher strain rates (1 s−1) due to incomplete DRX. Temperature increases from 900 °C to 1050 °C improve SRS via thermally activated dislocation annihilation, whereas temperatures above 1050 °C cause a sharp decrease in SRS due to abnormal grain coarsening and microstructural heterogeneity. The study identifies an optimal processing window (η > 0.40) for hot deforming Mn-Ni-Mo steel, with strain rates between 0.03 s−1 0.3 s−1 and temperatures from 1000 °C 1150 °C. The highest power dissipation efficiency (η ≈ 0.46) is observed at 1050 °C and 0.1 s−1, resulting in fine, equiaxed grains of 5 ± 2 μm.
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基于本构模型的Mn-Ni-Mo钢动态再结晶特性及工艺图绘制
反应器压力容器(rpv)的制造涉及一个复杂的多阶段锻造过程,该过程具有不同的应变、温度和应变速率,导致动态再结晶(DRX)、动态恢复和加工硬化。这些过程不断改变钢的微观结构,使预测其最终性能变得具有挑战性。本研究通过使用Gleeble 3500模拟器进行压缩试验,研究了Mn-Ni-Mo钢的热变形特性,从而解决了这一挑战。测试温度为900°C - 1200°C,应变速率为0.001 s−1 - 1 s−1。通过观察加工硬化速率、流动应力曲线和显微组织演变,研究了温度、应变速率和应变对DRX的影响。采用双曲正弦本构方程来模拟峰值应力、应变速率和变形温度之间的关系。结果表明,较高的变形温度或较低的应变速率降低了DRX的临界应变,增加了DRX的体积分数。钢的应变率敏感性(SRS)随应变和温度的变化而变化,在较低应变率(0.001 s−1和0.01 s−1)下变化显著,但在较高应变率(1 s−1)下由于DRX不完全而降低。温度从900°C升高到1050°C,通过热激活位错湮灭改善SRS,而温度高于1050°C,由于异常晶粒粗化和显微组织非均质性,SRS急剧下降。研究确定了最佳加工窗口(η >;0.40)适用于热变形的Mn-Ni-Mo钢,应变速率为0.03 s−1 ~ 0.3 s−1,温度为1000℃~ 1150℃。在1050℃和0.1 s−1的温度下,晶粒的功耗效率最高,η≈0.46,晶粒尺寸为5±2 μm。
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来源期刊
Materials Science and Engineering: A
Materials Science and Engineering: A 工程技术-材料科学:综合
CiteScore
11.50
自引率
15.60%
发文量
1811
审稿时长
31 days
期刊介绍: Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.
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