Evaluation on the mixing state of solid-liquid two-phase in stirred tank via an improved Voronoi diagram approach

IF 4.6 2区 工程技术 Q2 ENGINEERING, CHEMICAL Powder Technology Pub Date : 2025-03-15 Epub Date: 2025-01-06 DOI:10.1016/j.powtec.2025.120620
Qinwen Yao , Kai Yang , Xiaoxue Zhang , Wuliang Yin , Jianxin Pan , Hua Wang , Qingtai Xiao
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Abstract

In hydrometallurgical leaching of zinc-containing solid wastes, the poor performance of the solid-liquid two-phase mixing process could result in significant energy wastage. It was necessary to realize the assessment of the solid-liquid two-phase mixing state in the stirred tank to provide data support for the mixing process enhancement. In this work, the boundaryless problem of the traditional Voronoi diagram was solved by reconfiguring the boundary through virtual points, and a mixing uniformity assessment method was proposed in combination with the coefficient of variation method. Meanwhile, the mapping of image pixels to Voronoi cells was established, breaking through the limitation that the traditional camera technique could only be used for surface measurements, and realizing point measurements of solid-phase concentration distribution relationships. The evaluation results show that the uniformity of the four images with normal, circular, concentrated and Poisson distributions were 1.87, 1.50, 4.38 and 0.61, respectively. The uniformity of the mixing images for the similar model at the moments of 6.4, 10 and 11 s were 1.51, 1.25 and 0.38, respectively. The present method was very sensitive to the variation of the solid-phase distribution. Point measurements enabled qualitative and quantitative analysis of the spatial and temporal characteristics of particle concentrations. Qualitative analyses help to visualize changes in mixing conditions. The quantitative analysis helps to target improvements in the mixing process. In addition, the method could be extended to analyze flow and mixing processes with discrete geometrical features.

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用改进的Voronoi图法评价搅拌槽内固液两相的混合状态
在含锌固体废物湿法冶金浸出过程中,固液两相混合工艺性能较差,造成了较大的能源浪费。有必要实现搅拌槽内固液两相混合状态的评价,为改进搅拌过程提供数据支持。通过虚拟点重新配置边界,解决了传统Voronoi图的无边界问题,并结合变分系数法提出了混合均匀性评价方法。同时,建立了图像像素到Voronoi细胞的映射,突破了传统摄像技术只能用于表面测量的局限,实现了固相浓度分布关系的点测量。评价结果表明,正态分布、圆形分布、集中分布和泊松分布的图像均匀度分别为1.87、1.50、4.38和0.61。相似模型在6.4、10和11 s时刻的混合图像均匀度分别为1.51、1.25和0.38。该方法对固相分布的变化非常敏感。点测量可以对颗粒浓度的时空特征进行定性和定量分析。定性分析有助于可视化混合条件的变化。定量分析有助于有针对性地改进混合过程。此外,该方法还可以推广到具有离散几何特征的流动和混合过程的分析。
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来源期刊
Powder Technology
Powder Technology 工程技术-工程:化工
CiteScore
9.90
自引率
15.40%
发文量
1047
审稿时长
46 days
期刊介绍: Powder Technology is an International Journal on the Science and Technology of Wet and Dry Particulate Systems. Powder Technology publishes papers on all aspects of the formation of particles and their characterisation and on the study of systems containing particulate solids. No limitation is imposed on the size of the particles, which may range from nanometre scale, as in pigments or aerosols, to that of mined or quarried materials. The following list of topics is not intended to be comprehensive, but rather to indicate typical subjects which fall within the scope of the journal's interests: Formation and synthesis of particles by precipitation and other methods. Modification of particles by agglomeration, coating, comminution and attrition. Characterisation of the size, shape, surface area, pore structure and strength of particles and agglomerates (including the origins and effects of inter particle forces). Packing, failure, flow and permeability of assemblies of particles. Particle-particle interactions and suspension rheology. Handling and processing operations such as slurry flow, fluidization, pneumatic conveying. Interactions between particles and their environment, including delivery of particulate products to the body. Applications of particle technology in production of pharmaceuticals, chemicals, foods, pigments, structural, and functional materials and in environmental and energy related matters. For materials-oriented contributions we are looking for articles revealing the effect of particle/powder characteristics (size, morphology and composition, in that order) on material performance or functionality and, ideally, comparison to any industrial standard.
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