Experimental study on the mechanical and thermal properties of PEEK, CF/PEEK, and GF/PEEK thin-walled cylinders under static compressive tests

IF 5.7 1区 工程技术 Q1 ENGINEERING, CIVIL Thin-Walled Structures Pub Date : 2025-01-30 DOI:10.1016/j.tws.2025.113032
Shuyan Nie , Kunyong Guo , Yuanhao Tian , Liming Chen , Zhaoxin Yun , Xin Pan , Weiguo Li , Jie Wang , Xianbo Hou , Shaowei Zhu , Tao Liu , Zhenhua Song
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Abstract

Polyether ether ketone (PEEK) and its fiber reinforced composite thin-walled tube structures (TWCs) are widely used in engineering, but their mechanical properties under thermal conditions are rarely reported. In this paper, the static compressive mechanical properties of PEEK-TWCS, short glass fiber reinforced PEEK TWCS (GF/PEEK-TWCS) and short carbon fiber reinforced PEEK TWCS (CF/PEEK-TWCS) at 20 ℃ and 170 ℃ were investigated experimentally. The outcomes underscore that the compressive strength, specific energy absorption and stiffness of the cylinders are significant sensitive to temperature, with PEEK-TWCS demonstrating the highest sensitivity, exhibiting a reduction of over 75 % at 170 °C. Comparatively, the reinforcing effects of carbon fibers and glass fibers are markedly pronounced at 170 °C, substantially ameliorating the mechanical performance of the cylindrical structures. Utilizing a 3D-Digital Image Correlation (DIC) optical strain measurement system, an inhomogeneous strain distribution in the elastic phase was observed for all materials, with increasing compression, a buckling half-wave formed, leading to localized buckling. According to the micro-nano electron computed tomography scanner (Nano-CT), the plasticity of GF/PEEK-TWCS is better than that of CF/PEEK-TWCS and PEEK-TWCS at 20 °C. In addition, microscopic fracture surface analysis revealed that the ductile matrix behavior in CF/PEEK, juxtaposed with brittle fiber fracture, indicative of interface damage and fiber pull-out. In contrast, PEEK displayed brittle fracture characteristics. This research provides support for the temperature-dependent mechanical behavior of PEEK-based composites, offering a foundation for the development of advanced materials for high-temperature applications.

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聚醚醚酮(PEEK)及其纤维增强复合材料薄壁管结构(TWCs)被广泛应用于工程领域,但其在热条件下的力学性能却鲜有报道。本文通过实验研究了 PEEK-TWCS、短玻璃纤维增强 PEEK TWCS(GF/PEEK-TWCS)和短碳纤维增强 PEEK TWCS(CF/PEEK-TWCS)在 20 ℃ 和 170 ℃ 下的静态压缩力学性能。结果表明,圆柱体的抗压强度、比能量吸收和刚度对温度非常敏感,其中 PEEK-TWCS 的敏感性最高,在 170 ℃ 时降低了 75% 以上。相比之下,碳纤维和玻璃纤维在 170 °C 时的增强效果明显,大大改善了圆柱形结构的机械性能。利用三维数字图像相关(DIC)光学应变测量系统,观察到所有材料在弹性阶段的应变分布不均匀,随着压缩量的增加,形成了屈曲半波,导致局部屈曲。根据微纳电子计算层析成像扫描仪(Nano-CT)的结果,在 20 °C 时,GF/PEEK-TWCS 的塑性优于 CF/PEEK-TWCS 和 PEEK-TWCS。此外,显微断裂面分析表明,CF/PEEK 的韧性基体行为与脆性纤维断裂并存,表明存在界面损伤和纤维拉出。相比之下,PEEK 显示出脆性断裂特征。这项研究为基于 PEEK 的复合材料随温度变化的机械行为提供了支持,为开发高温应用的先进材料奠定了基础。
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来源期刊
Thin-Walled Structures
Thin-Walled Structures 工程技术-工程:土木
CiteScore
9.60
自引率
20.30%
发文量
801
审稿时长
66 days
期刊介绍: Thin-walled structures comprises an important and growing proportion of engineering construction with areas of application becoming increasingly diverse, ranging from aircraft, bridges, ships and oil rigs to storage vessels, industrial buildings and warehouses. Many factors, including cost and weight economy, new materials and processes and the growth of powerful methods of analysis have contributed to this growth, and led to the need for a journal which concentrates specifically on structures in which problems arise due to the thinness of the walls. This field includes cold– formed sections, plate and shell structures, reinforced plastics structures and aluminium structures, and is of importance in many branches of engineering. The primary criterion for consideration of papers in Thin–Walled Structures is that they must be concerned with thin–walled structures or the basic problems inherent in thin–walled structures. Provided this criterion is satisfied no restriction is placed on the type of construction, material or field of application. Papers on theory, experiment, design, etc., are published and it is expected that many papers will contain aspects of all three.
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Editorial Board Mechanics of finite nonlinear viscoelastic growth for soft biological tissues Comparative analysis of damage and energy absorption mechanisms in various plain-weave fiber reinforced composites under multi-angle low-velocity impact Editorial Board Experimental study on the mechanical and thermal properties of PEEK, CF/PEEK, and GF/PEEK thin-walled cylinders under static compressive tests
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