Mechanisms for pore evolution and heterogeneity in laser powder bed fusion aluminum elucidated through x-ray microscopy

IF 2.9 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Materialia Pub Date : 2025-03-01 Epub Date: 2025-02-04 DOI:10.1016/j.mtla.2025.102358
Daniel R. Sinclair, Nikhilesh Chawla
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Abstract

Laser powder bed fusion (LPBF) of metallic components produces a unique combination of thermomechanical phenomena such as convection, vaporization, and keyholing. The resulting melt pool structure is not easily characterized in post-facto analysis of printed parts, making process-structure correlations very difficult. Here, structures produced by laser keyhole formation during LPBF of an aerospace aluminum alloy were studied through a simplified sample geometry and controlled remelting. The final distribution of pores within the solidified wall were imaged and quantified through high resolution x-ray microscopy and correlated to the remelted melt pool structure. Based on observations from this multimodal, quantitative analysis, a mechanism for the distribution of porosity is proposed. Novel effects of laser processing conditions on microstructures are thus described, highlighting a key source of heterogeneity across the scales of melt pools to thin 3D features.

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用x射线显微镜研究激光粉末床熔铝的孔隙演化和非均质性机制
激光粉末床熔融(LPBF)的金属部件产生一个独特的组合热机械现象,如对流,汽化,和钥匙孔。由此产生的熔池结构在打印部件的事后分析中不容易表征,使得过程结构相关性非常困难。通过简化样品几何形状和控制重熔,研究了航空航天铝合金LPBF过程中激光锁孔形成的结构。通过高分辨率x射线显微镜对凝固壁内气孔的最终分布进行了成像和量化,并与重熔熔池结构进行了关联。基于这种多模态的定量分析,提出了孔隙度分布的机制。因此,描述了激光加工条件对微观结构的新影响,突出了跨熔池尺度到薄3D特征的非均质性的关键来源。
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来源期刊
Materialia
Materialia MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
6.40
自引率
2.90%
发文量
345
审稿时长
36 days
期刊介绍: Materialia is a multidisciplinary journal of materials science and engineering that publishes original peer-reviewed research articles. Articles in Materialia advance the understanding of the relationship between processing, structure, property, and function of materials. Materialia publishes full-length research articles, review articles, and letters (short communications). In addition to receiving direct submissions, Materialia also accepts transfers from Acta Materialia, Inc. partner journals. Materialia offers authors the choice to publish on an open access model (with author fee), or on a subscription model (with no author fee).
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