Fracture experiments of coated and non-coated epoxy-alumina composites coupled with micro-CT

IF 8.1 2区 材料科学 Q1 ENGINEERING, MANUFACTURING Composites Part A: Applied Science and Manufacturing Pub Date : 2025-05-01 Epub Date: 2025-01-31 DOI:10.1016/j.compositesa.2025.108762
Yichun Tang , Yanran Wang , Michael C. Hillman , Jiun-Shyan Chen , Jing Du
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Abstract

Polymer-ceramic composites are widely used in electronic devices, biomedical engineering and other applications. This paper presents the results of an experimental study on the effects of silane coating on the fracture properties of epoxy-alumina composite. Mechanical testing coupled with micro X-ray computed tomography (micro-CT) was performed to investigate epoxy-alumina composite’s fracture behaviors. The matrix-particle interface was shown to be the weakest link in non-coated composites. Guided by the discovery, silane coating was applied to the particles to enhance the matrix-particle interfacial adhesion. The occurrence of matrix-particle interface debonding was reduced and delayed for composites with silane treatment on the particle surfaces. Ultimately, the fracture toughness and crack growth resistance of the composites were improved.

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涂层与非涂层环氧-氧化铝复合材料耦合微ct断裂实验
聚合物-陶瓷复合材料广泛应用于电子器件、生物医学工程等领域。本文介绍了硅烷涂层对环氧氧化铝复合材料断裂性能影响的实验研究结果。采用力学测试结合微x射线计算机断层扫描(micro- ct)技术研究了环氧氧化铝复合材料的断裂行为。在非涂层复合材料中,基体-颗粒界面是最薄弱的环节。在这一发现的指导下,硅烷涂层被涂在颗粒上以增强基质-颗粒界面的附着力。在颗粒表面进行硅烷处理可以减少和延缓复合材料基体-颗粒界面脱粘的发生。最终提高了复合材料的断裂韧性和抗裂纹扩展能力。
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来源期刊
Composites Part A: Applied Science and Manufacturing
Composites Part A: Applied Science and Manufacturing 工程技术-材料科学:复合
CiteScore
15.20
自引率
5.70%
发文量
492
审稿时长
30 days
期刊介绍: Composites Part A: Applied Science and Manufacturing is a comprehensive journal that publishes original research papers, review articles, case studies, short communications, and letters covering various aspects of composite materials science and technology. This includes fibrous and particulate reinforcements in polymeric, metallic, and ceramic matrices, as well as 'natural' composites like wood and biological materials. The journal addresses topics such as properties, design, and manufacture of reinforcing fibers and particles, novel architectures and concepts, multifunctional composites, advancements in fabrication and processing, manufacturing science, process modeling, experimental mechanics, microstructural characterization, interfaces, prediction and measurement of mechanical, physical, and chemical behavior, and performance in service. Additionally, articles on economic and commercial aspects, design, and case studies are welcomed. All submissions undergo rigorous peer review to ensure they contribute significantly and innovatively, maintaining high standards for content and presentation. The editorial team aims to expedite the review process for prompt publication.
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