Multipurpose DIY Spectrophotometer for Teaching Analytical Chemistry

IF 2.9 3区 教育学 Q2 CHEMISTRY, MULTIDISCIPLINARY Journal of Chemical Education Pub Date : 2025-01-16 DOI:10.1021/acs.jchemed.4c01229
Gina DelMonache, Pratahdeep Gogoi, Xiaoli Ge, Xingyu Wang, Rachel Snider, Owen Szeglowski, Timothy R. Cook, Ziyun Wang and Yuguang C. Li*, 
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Abstract

Spectroscopy is an integral part of chemical research, and the operation of any spectroscopic instrument is critical in chemical education. This study presents a low-cost, do-it-yourself (DIY) style spectrophotometer system that can be adapted for UV–vis spectrophotometry, fluorimetry, and atomic emission spectroscopy applications. The DIY system is constructed with commonly available hardware and 3D-printed parts, totaling less than $100 USD. Python code is also provided to process the color spectrum image into intensity vs wavelength data, similar to any commercial-level instrument. The functionality of the DIY spectrophotometer is demonstrated with the absorption of KMnO4, fluorescence of fluorescein and atomic emission of LiCl, NaCl, BaCl2, and SrCl2. All of the collected spectra show accurate results compared to a commercial instrument or existing literature. The goal of this project is to provide a hands-on platform for undergraduate students to see and modify the individual components of a spectrophotometer, which will enhance their understanding of the underlying principles.

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多用途DIY分光光度计教学分析化学
光谱学是化学研究的一个组成部分,任何光谱仪器的操作在化学教育中都是至关重要的。本研究提出了一种低成本,自己动手(DIY)风格的分光光度计系统,可适用于紫外-可见分光光度计,荧光法和原子发射光谱应用。该DIY系统由常见的硬件和3d打印部件组成,总计不到100美元。还提供了Python代码来将彩色光谱图像处理为强度与波长数据,类似于任何商业级仪器。通过对KMnO4的吸收、荧光素的荧光以及LiCl、NaCl、BaCl2和SrCl2的原子发射,证明了自制分光光度计的功能。与商业仪器或现有文献相比,所有收集到的光谱显示准确的结果。该项目的目标是为本科生提供一个动手平台,以查看和修改分光光度计的各个组件,这将增强他们对基本原理的理解。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Journal of Chemical Education
Journal of Chemical Education 化学-化学综合
CiteScore
5.60
自引率
50.00%
发文量
465
审稿时长
6.5 months
期刊介绍: The Journal of Chemical Education is the official journal of the Division of Chemical Education of the American Chemical Society, co-published with the American Chemical Society Publications Division. Launched in 1924, the Journal of Chemical Education is the world’s premier chemical education journal. The Journal publishes peer-reviewed articles and related information as a resource to those in the field of chemical education and to those institutions that serve them. JCE typically addresses chemical content, activities, laboratory experiments, instructional methods, and pedagogies. The Journal serves as a means of communication among people across the world who are interested in the teaching and learning of chemistry. This includes instructors of chemistry from middle school through graduate school, professional staff who support these teaching activities, as well as some scientists in commerce, industry, and government.
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