Multi-class food additives determination in food and beverages from the Czech market by UPLC-MS/MS.

IF 2.5 3区农林科学 Q2 CHEMISTRY, APPLIED Food additives & contaminants. Part B, Surveillance Pub Date : 2025-06-01 Epub Date: 2025-02-10 DOI:10.1080/19393210.2025.2461488

Aliaksandra Kharoshka, Jana Hajslova, Vera Schulzova

引用次数: 0

Abstract

While the use of food additives is common manufacturing practice, the levels used in food have to be compliant with the prescribed legislation. For fast control of present levels of food additives in products, ultra-high performance liquid chromatography coupled to tandem mass spectrometry with a triple quadrupole linear ion trap (QTRAP) mass analyser was applied to develop a method for the simultaneous determination of 41 frequently added food additives and flavourings, including 16 water-soluble colourants, 14 illegal dyes, 7 sweeteners, 2 preservatives, and 2 purine alkaloids. The method was validated using energy drink, chilli powder, condiment, and jelly sweets as food sample matrices. The average recovery values were in the range of 70‒120%, and the relative standard deviations were less than 10% for the majority of the analytes. The validated method was applied for the analysis of 134 samples from the Czech market.

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捷克市场食品和饮料中多类食品添加剂的UPLC-MS/MS测定。

虽然使用食品添加剂是常见的生产做法，但食品中使用的含量必须符合规定的法规。为了快速控制产品中食品添加剂的含量，采用超高效液相色谱-串联质谱联用三重四极杆线性离子阱（QTRAP）质谱分析仪，建立了一种同时检测41种常见食品添加剂和调味料的方法，包括16种水溶性着色剂、14种非法染料、7种甜味剂、2种防腐剂和2种嘌呤生物碱。以能量饮料、辣椒粉、调味品和果冻糖果为食品样品基质，对该方法进行了验证。平均回收率在70 ~ 120%之间，相对标准偏差小于10%。应用该方法对来自捷克市场的134份样品进行了分析。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Food additives & contaminants. Part B, Surveillance 农林科学-毒理学

CiteScore

5.30

自引率

10.30%

发文量

审稿时长

2.7 months

期刊介绍： Food Additives & Contaminants: Part B publishes surveillance data indicating the presence and levels of occurrence of designated food additives, residues and contaminants in foods, food supplements and animal feed. Data using validated methods must meet stipulated quality standards to be acceptable and must be presented in a prescribed format for subsequent data-handling. Food Additives & Contaminants: Part B restricts its scope to include certain classes of food additives, residues and contaminants. This is based on a goal of covering those areas where there is a need to record surveillance data for the purposes of exposure and risk assessment. The scope is initially restricted to: Additives - food colours, artificial sweeteners, and preservatives; Residues – veterinary drug and pesticide residues; Contaminants – metals, mycotoxins, phycotoxins, plant toxins, nitrate/nitrite, PCDDs/PCFDs, PCBs, PAHs, acrylamide, 3-MPCD and contaminants derived from food packaging. Readership: The readership includes scientists involved in all aspects of food safety and quality and particularly those involved in monitoring human exposure to chemicals from the diet. Papers reporting surveillance data in areas other than the above should be submitted to Part A . The scope of Part B will be expanded from time-to-time to ensure inclusion of new areas of concern.