Quantitative Estimation of the Characteristic Grain Sizes of Laboratory Rock Samples by the Broadband Optoacoustic Spectroscopy Method

IF 1 4区 地球科学 Q4 GEOCHEMISTRY & GEOPHYSICS Izvestiya, Physics of the Solid Earth Pub Date : 2025-02-20 DOI:10.1134/S1069351324701003
N. B. Podymova, A. V. Ponomarev, P. A. Kaznacheev, T. E. Baghdasaryan, M. A. Matveev, G. S. Indakov
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Abstract—A technique for quantitative estimation of characteristic grain sizes in laboratory rock samples using the relationship between the frequency and attenuation of longitudinal ultrasonic waves in the samples is proposed and implemented experimentally. This relationship is quantified using broadband optoacoustic spectroscopy with a laser source of ultrasound and piezoelectric registration of nanosecond ultrasonic pulses in the operating frequency range of 1–70 MHz. The application of the theoretical model of ultrasound scattering in single-phase polycrystalline materials to quantitative estimation of the maximum and average grain sizes in multiphase rocks is shown using five samples of metasandstones of zonally metamorphosed Ladoga series of the Paleoproterozoic of the Baltic Shield, which underwent different degrees of structural and textural transformations during ancient metamorphic events. The reliability of the data obtained using broadband optoacoustic spectroscopy was for the first time confirmed by independent scanning electron microscopy of the polished surfaces of all samples. The average and maximum grain sizes were estimated separately using the conventional method of line crossing from optical micrographs of thin sections performed for two selected samples, which also showed good agreement with the acoustic spectroscopy data. The proposed method of broadband optoacoustic spectroscopy for estimation of characteristic grain sizes of laboratory rock samples can be used to analyze the possible relationship between their structural features and thermobaric conditions of formation.

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宽带光声光谱法定量估计实验室岩石样品的特征粒度
摘要:提出了一种利用纵波频率与衰减之间的关系定量估计岩样特征粒度的方法,并进行了实验实现。这种关系是量化使用宽带光声光谱与激光源超声和压电配准纳秒超声脉冲在工作频率范围为1-70 MHz。本文以波罗的海地盾古元古代拉多加系带状变质变质的5块变质砂岩为研究对象,介绍了单相多晶材料超声散射理论模型在多相岩石中最大晶粒尺寸和平均晶粒尺寸定量估计中的应用。通过对所有样品抛光表面的独立扫描电镜,首次证实了宽带光声光谱数据的可靠性。利用传统的交叉法对两个样品的薄片光学显微图分别估计了平均和最大晶粒尺寸,这也与声学光谱数据吻合得很好。本文提出的宽带光声光谱法估算实验室岩样特征粒度的方法可用于分析其结构特征与地层热压条件之间可能存在的关系。
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来源期刊
Izvestiya, Physics of the Solid Earth
Izvestiya, Physics of the Solid Earth 地学-地球化学与地球物理
CiteScore
1.60
自引率
30.00%
发文量
60
审稿时长
6-12 weeks
期刊介绍: Izvestiya, Physics of the Solid Earth is an international peer reviewed journal that publishes results of original theoretical and experimental research in relevant areas of the physics of the Earth''s interior and applied geophysics. The journal welcomes manuscripts from all countries in the English or Russian language.
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