Inconel 625/NiCrWMo functionally graded materials manufactured by direct laser deposition

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-02-20 DOI:10.1016/j.matchar.2025.114862
André A. Ferreira , Ana R. Reis , João P. Sousa , João M. Cruz , Manuel F. Vieira
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Abstract

The production of functional gradient materials (FGM) is an option for the various industrial sectors and a solution for many engineering applications. FGM's are a class of materials that can also be characterised as metal composites that gradually change composition and structure. In this study, the production of FGM's on 42CrMo4 structural steel substrate, varying the composition from 100 % Inconel 625 to 100 % NiCrWMo alloy, was successfully fabricated using the Direct Laser Deposition technique. The substrate was pre-heated to decrease the cooling rate and the formation of metastable phases of the heat-affected zone, and for comparison purposes, deposition was performed on the substrate without pre-heating. A mixture of Inconel 625 and NiCrWMo-type nickel superalloy powders was used to produce functionally graded structures. Microstructural characterisation and phase identification were performed by scanning electron microscopy, chemical analyses by energy-dispersive x-ray spectroscopy and electron backscatter diffraction. Microhardness mapping performed on the FGMs allowed the hardness profile along the gradient to be evaluated and correlated with the chemical analyses to be performed. The metallurgical, chemical, and mechanical characterisations and the correlation with process parameters are determined and discussed throughout this investigation. This research shows an innovative FGM, which has not yet been produced, allowing this research to evaluate the characteristics of each powder's mixture composition. It was also possible to observe the effect of alloying elements on the microstructure and hardness of the graded materials.
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直接激光沉积制备Inconel 625/NiCrWMo功能梯度材料
功能梯度材料(FGM)的生产是各种工业部门的一种选择,也是许多工程应用的解决方案。FGM是一类也可以被描述为逐渐改变成分和结构的金属复合材料的材料。在本研究中,利用直接激光沉积技术成功地在42CrMo4结构钢基体上制备了FGM,其成分从100% Inconel 625到100% NiCrWMo合金不等。为了降低冷却速度和热影响区亚稳相的形成,对衬底进行了预热,为了比较,在衬底上进行了不预热的沉积。采用Inconel 625和nicrwmo型镍高温合金混合粉末制备功能梯度组织。通过扫描电镜进行了显微结构表征和物相鉴定,通过能量色散x射线能谱和电子背散射衍射进行了化学分析。在fgm上进行显微硬度映射,可以评估沿梯度的硬度分布图,并与要进行的化学分析相关联。在整个研究过程中,确定并讨论了冶金、化学和机械特性以及与工艺参数的相关性。这项研究展示了一种尚未生产的创新女性生殖器切割,使这项研究能够评估每种粉末混合物组成的特性。还可以观察到合金元素对梯度材料显微组织和硬度的影响。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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