Study on the strength-plasticity enhancement mechanism of the SiCp/Fe symmetric gradient structure and alloying in the high-particle-content layer

IF 7 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Science and Engineering: A Pub Date : 2025-05-01 Epub Date: 2025-03-04 DOI:10.1016/j.msea.2025.148140
Wen-quan Li , Zheng-yu Zhong , Ning-zhi Zheng , Kai-yao Wang , Ying Guo , Chao Zhang
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Abstract

The construction of heterogeneous structures is an effective method to achieve a favorable balance between material strength and ductility. By controlling the silicon carbide (SiCp) particle content, Fe-based layered composites with a symmetric gradient structure were prepared using spark plasma sintering (SPS) and subjected to hot rolling to investigate the microstructural evolution and mechanical performance of each layer. The results show that the gradient distribution of SiCp content leads to different grain sizes across the layers. The formation of an amorphous layer between SiCp and Fe, as well as FeSiO3 crystalline products, promoted strong bonding between the two. The gradient distribution of SiCp content resulted in a symmetric gradient in Vickers hardness values across the material. Compared with pure Fe, homogeneous 3 % SiCp/Fe, and 10 % SiCp/Fe composites, the SiCp/Fe symmetric gradient structure exhibited higher hardness without a significant reduction in plasticity. After hot rolling, the yield strength of the SiCp/Fe symmetric gradient structure reached 912.45 MPa, with an elongation of 7.67 %. In this study, the strength and plasticity of the symmetric gradient structure were enhanced by 178.10 % and 56.53 %, respectively, compared with the Fe-8Cr-4.5Ni structure prepared by SPS. This demonstrated the synergistic enhancement effect of the symmetric gradient design on strength and plasticity. Additionally, due to the high localized stresses during the hot rolling process, SiCp in the 10 % SiCp/Fe layer was decomposed and reacted with the Fe matrix to form Fe-C and Fe-Si compounds. The ultrafine grains in this layer also contributed to the high strength of material.
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高颗粒层SiCp/Fe对称梯度结构及合金化的强度塑性增强机理研究
非均质结构的施工是实现材料强度与延性良好平衡的有效方法。通过控制碳化硅(SiCp)颗粒含量,采用火花等离子烧结(SPS)法制备了具有对称梯度结构的铁基层状复合材料,并对其进行热轧,研究了各层的显微组织演变和力学性能。结果表明,SiCp含量的梯度分布导致了不同层间晶粒尺寸的变化。在SiCp和Fe之间形成非晶层,以及FeSiO3晶体产物,促进了两者之间的强结合。SiCp含量的梯度分布导致整个材料的维氏硬度值呈对称梯度。与纯铁、均相3% SiCp/Fe和10% SiCp/Fe复合材料相比,SiCp/Fe对称梯度结构具有更高的硬度,但塑性没有明显降低。经热轧后,SiCp/Fe对称梯度组织的屈服强度达到912.45 MPa,伸长率为7.67%。与SPS制备的Fe-8Cr-4.5Ni结构相比,对称梯度结构的强度和塑性分别提高了178.10%和56.53%。这证明了对称梯度设计对强度和塑性的协同增强作用。此外,由于热轧过程中的高局部应力,10% SiCp/Fe层中的SiCp被分解并与Fe基体反应生成Fe- c和Fe- si化合物。该层中的超细晶粒也有助于材料的高强度。
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来源期刊
Materials Science and Engineering: A
Materials Science and Engineering: A 工程技术-材料科学:综合
CiteScore
11.50
自引率
15.60%
发文量
1811
审稿时长
31 days
期刊介绍: Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.
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