Plasma evolution investigation and aging grade evaluation of heat resistant steel based on laser induced plasma images†

IF 3.1 2区 化学 Q2 CHEMISTRY, ANALYTICAL Journal of Analytical Atomic Spectrometry Pub Date : 2025-01-22 DOI:10.1039/D4JA00368C
Junbin Cai, Meirong Dong, Feiqiang Tang, Kaiqing Chen, Zhichun Li, Weijie Li, Shunchun Yao and Jidong Lu
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Abstract

The accurate evaluation of heat-resistant steel deterioration using laser-induced breakdown spectroscopy (LIBS) is of great importance for the safe operation of high-temperature pressure equipment. Understanding how plasma expresses matrix properties and utilizing plasma information effectively can lead to achieving more effective detection methods. In this study, the plasma evolution and pulse fluctuations of typical heat-resistant steel T91 are studied based on plasma images to understand the different evolution stages and characteristics of plasma. T91 specimens with different aging grades are employed to investigate the expression form, evolution and identification of matrix information on plasma. Subsequently, the plasma images and the RSD images based on pulse–pulse relative standard deviation (RSD) were employed to build an aging grade evaluation model, the best model accuracies were 96.6% and 96.0%, respectively. A model combining these two image features achieved the highest accuracy at 99.8%. Finally, the effects of the delay time, region selection, and data coupling strategy on model performance were explored. The results indicate that the temporal–spatial characteristics, identification, and stability of plasma information have a significant effect on the performance of the model. This study deepens the understanding of the plasma evolution and matrix effect of heat-resistant steel and expands the application of plasma image information for property detection.

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基于激光诱导等离子体图像的耐热钢等离子体演化研究及老化等级评定
利用激光诱导击穿光谱(LIBS)准确评价耐热钢劣化对高温承压设备的安全运行具有重要意义。了解等离子体如何表达基质特性和有效利用等离子体信息可以实现更有效的检测方法。本研究基于等离子体图像研究典型耐热钢T91的等离子体演化和脉冲波动,了解等离子体的不同演化阶段和特征。采用不同老化等级的T91标本,研究血浆中基质信息的表达形式、演变及鉴定。随后,利用等离子体图像和基于脉冲相对标准偏差(RSD)的RSD图像构建了老化等级评价模型,模型的最佳准确率分别为96.6%和96.0%。结合这两个图像特征的模型达到了99.8%的最高准确率。最后,探讨了延迟时间、区域选择和数据耦合策略对模型性能的影响。结果表明,等离子体信息的时空特性、识别性和稳定性对模型的性能有重要影响。本研究加深了对耐热钢等离子体演化和基体效应的认识,拓展了等离子体图像信息在耐热钢性能检测中的应用。
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来源期刊
CiteScore
6.20
自引率
26.50%
发文量
228
审稿时长
1.7 months
期刊介绍: Innovative research on the fundamental theory and application of spectrometric techniques.
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