Enhanced intragranular precipitation strengthening in Sc-microalloyed ultrafine-grained SiCp/Al-Cu-Mg composites via retrogression and re-ageing heat treatment

IF 7.9 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials & Design Pub Date : 2025-03-01 DOI:10.1016/j.matdes.2025.113789
Yunpeng Cai, Kan Liu, Yiwei Dong, Andong Hua, Yishi Su, Qiubao Ouyang, Di Zhang
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Abstract

Ultrafine-grained Al matrix composites suffer from the insufficient dislocation accumulation capability and intragranular precipitation strengthening due to their length-scale dependent precipitation behaviors. In this work, a combination of Sc-microalloying and a retrogression and re-ageing (RRA) route was applied on the SiCp/Al-Cu-Mg composites to achieve well-balanced strength and ductility. Compared to the T6 treatment, RRA heat treatment exhibit a significant strengthening effect in Sc-microalloyed composites with only a slight loss in ductility. The yield strength and ultimate strength of the Sc-RRA samples reach up to 686.4 MPa and 734.5 MPa, respectively. The plastic deformation mechanism was analyzed by thermal activation analysis and TEM observation of deformed microstructure. The plastic deformation of UFG composites, both with and without Sc, is primarily governed by a dislocation-grain boundary interaction mechanism. As confirmed by the observed stacking faults, the Sc-microalloyed composite subjected to T6 treatment suffers from poor dislocation storge capacity and insufficient intragranular precipitation strengthening. In contrast, the RRA treatment promotes the formation of intragranular Al3Sc precipitates and GP zones, which improve the dislocation accumulation capability and precipitation strengthening of ultrafine-grained composites by pinning dislocations. This work provides an accessible pathway to exploit aluminum matrix composites with advanced strength-ductility balance.

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通过回火和再时效热处理增强sc微合金化超细晶SiCp/Al-Cu-Mg复合材料的晶内析出强化
超细晶Al基复合材料由于其长度尺度依赖性的析出行为,导致其位错积累能力和晶内析出强化能力不足。在这项工作中,将sc微合金化和回退再时效(RRA)相结合的方法应用于SiCp/Al-Cu-Mg复合材料,以获得良好的强度和塑性平衡。与T6处理相比,RRA热处理在sc微合金复合材料中表现出明显的强化效果,而塑性损失很小。Sc-RRA试样的屈服强度和极限强度分别达到686.4 MPa和734.5 MPa。通过热活化分析和变形显微组织的透射电镜观察,分析了塑性变形机理。含Sc和不含Sc的UFG复合材料的塑性变形主要由位错-晶界相互作用机制控制。观察到的层错证实,经T6处理的sc微合金复合材料位错储存能力差,晶内析出强化不足。相反,RRA处理促进了晶内Al3Sc相和GP区的形成,通过钉住位错提高了超细晶复合材料的位错积累能力和沉淀强化能力。本研究为开发具有先进强度-延性平衡的铝基复合材料提供了一条可行的途径。
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来源期刊
Materials & Design
Materials & Design Engineering-Mechanical Engineering
CiteScore
14.30
自引率
7.10%
发文量
1028
审稿时长
85 days
期刊介绍: Materials and Design is a multi-disciplinary journal that publishes original research reports, review articles, and express communications. The journal focuses on studying the structure and properties of inorganic and organic materials, advancements in synthesis, processing, characterization, and testing, the design of materials and engineering systems, and their applications in technology. It aims to bring together various aspects of materials science, engineering, physics, and chemistry. The journal explores themes ranging from materials to design and aims to reveal the connections between natural and artificial materials, as well as experiment and modeling. Manuscripts submitted to Materials and Design should contain elements of discovery and surprise, as they often contribute new insights into the architecture and function of matter.
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