High-temperature deformation behaviour of coarse-grained and fine-grained magnesium sheets: Insights from processing maps and constitutive modelling

IF 4.7 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Chemistry and Physics Pub Date : 2025-07-01 Epub Date: 2025-03-05 DOI:10.1016/j.matchemphys.2025.130679
Smarajit Punay Kanti, B.N. Sahoo
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Abstract

In recent years, magnesium (Mg) sheets have emerged as a prominent structural material in the transportation and aerospace industries, where they are exposed to significant mechanical and thermal stresses. To enhance their performance, it is critical to define optimal workability zones across different temperatures and strain rates, particularly for highly deformed Mg sheets. This study investigates high-temperature deformation behavior of coarse-grained (CG) and fine-grained (FG) AZ31 Mg alloy sheets produced through novel hot rolling (HR) process with 40 % thickness reduction per pass. The HR process reduced the grain size in FG materials to 8 μm, compared to an initial grain size of 160 μm in CG materials. The deformation characteristics were evaluated through a constitutive model that includes flow stress, deformation activation energy, and processing maps over a range of strain rates (0.001–10 s−1) and temperatures (250 °C-450 °C). Processing maps identified both stable and instable zones during high-temperature tensile deformation, with dynamic recovery (DRV) governing stable regions of CG, while dislocation climb drives FG Mg sheet. The instability was marked by twinning, stress localization, and cracking for both materials. The FG Mg sheet exhibited a lower average activation energy (144 kJ/mol) than the CG material (156 kJ/mol). A comprehensive microstructural analysis using EBSD, SEM, and TEM provided visual validation of deformation mechanisms predicted by the constitutive model and processing maps.
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粗粒和细粒镁片的高温变形行为:从加工图和本构建模的见解
近年来,镁(Mg)片已成为一种突出的结构材料,在运输和航空航天工业,他们暴露在显著的机械和热应力。为了提高其性能,在不同温度和应变速率下定义最佳可加工区是至关重要的,特别是对于高度变形的Mg板。研究了采用新型热轧工艺(HR)生产的粗晶(CG)和细晶(FG) AZ31镁合金板材的高温变形行为,每道次减厚40%。HR工艺将FG材料的晶粒尺寸减小到8 μm,而CG材料的初始晶粒尺寸为160 μm。变形特性通过本构模型进行评估,该模型包括流动应力、变形激活能和应变率(0.001-10 s−1)和温度(250°C-450°C)范围内的加工图。加工图确定了高温拉伸变形过程中的稳定区和不稳定区,动态恢复(DRV)控制CG的稳定区,而位错爬升驱动FG - Mg片。两种材料的不稳定性表现为孪晶、应力局部化和开裂。FG - Mg材料的平均活化能(144 kJ/mol)低于CG材料的平均活化能(156 kJ/mol)。利用EBSD, SEM和TEM进行全面的微观结构分析,为本构模型和加工图预测的变形机制提供了视觉验证。
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来源期刊
Materials Chemistry and Physics
Materials Chemistry and Physics 工程技术-材料科学:综合
CiteScore
8.70
自引率
4.30%
发文量
1515
审稿时长
69 days
期刊介绍: Materials Chemistry and Physics is devoted to short communications, full-length research papers and feature articles on interrelationships among structure, properties, processing and performance of materials. The Editors welcome manuscripts on thin films, surface and interface science, materials degradation and reliability, metallurgy, semiconductors and optoelectronic materials, fine ceramics, magnetics, superconductors, specialty polymers, nano-materials and composite materials.
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