Drawing of tungsten fiber tows impregnated with Al/Epoxy matrix composites: Interfacial bonding and failure

IF 9.8 1区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Composites Science and Technology Pub Date : 2025-05-26 Epub Date: 2025-03-08 DOI:10.1016/j.compscitech.2025.111140
Zhenhui He , Enling Tang , Wenjin Yao , Ruizhi Wang
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Abstract

The most widely used high-performance resin matrix composites generally follow the microparticle-fiber-epoxy resin system structure. However, due to the difference in material properties of each component, the failure of fiber-reinforced resin matrix composites is often caused by its internal load inhomogeneity. In this paper, digital image technology is used to quantify the micro-failure form of the interface between fiber and epoxy resin matrix based on droplet solidification experiment and tungsten fiber impregnation tensile experiment. The upper and lower limits of coupling between fibers in fiber-reinforced polymer matrix composites were quantified, and a universal prediction method for the strength of fiber-reinforced particle-doped resin matrix composites was developed. The research results show that: A small amount of Al particles inclusion can enhance the affinity between the epoxy resin matrix and the tungsten material, thereby improving the mechanical properties of the fiber reinforced resin matrix material. When the amount of aluminum particles is 15 vol%, the viscous flow performance of the epoxy resin is similar to that of the pure epoxy resin. The load-bearing efficiency will be generated by the mutual nesting at the interface in the epoxy resin-tungsten fiber structure, where the maximum insertion depth is 9.08 μm and the average insertion depth is 4.69 μm. The maximum tensile load shows a trend of increasing first and then decreasing with the increase of aluminum particle volume content, reaching its maximum value at a volume inclusion of 40 vol%. The closer the epoxy resin matrix to the fiber, the greater the effect on the interfacial chelation effect, in which the effective interphase thickness is 0.128 times the fiber radius. The energy absorption of pure epoxy resin-single fiber bonding phase is 138.45 MJ/m3, while the energy absorption of the effective bonding area between epoxy matrix and tungsten fiber is between 76.52–224.95 MJ/m3 when aluminum particles are mixed.

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Al/环氧基复合材料浸渍钨纤维束的拉伸:界面结合和失效
目前应用最广泛的高性能树脂基复合材料一般遵循微粒-纤维-环氧树脂体系结构。然而,由于各组分材料性能的差异,纤维增强树脂基复合材料的失效往往是由其内部载荷的不均匀性引起的。本文在液滴凝固实验和钨纤维浸渍拉伸实验的基础上,采用数字图像技术定量分析了纤维与环氧树脂基体界面的微观破坏形式。量化了纤维增强聚合物基复合材料中纤维间耦合的上下限,建立了一种通用的纤维增强颗粒掺杂树脂基复合材料强度预测方法。研究结果表明:少量Al颗粒的夹杂可以增强环氧树脂基体与钨材料之间的亲和力,从而改善纤维增强树脂基体材料的力学性能。当铝颗粒掺量为15 vol%时,环氧树脂的粘性流动性能与纯环氧树脂相似。环氧树脂-钨纤维结构界面处的互嵌套将产生承载效率,其中最大嵌套深度为9.08 μm,平均嵌套深度为4.69 μm。随着铝颗粒体积含量的增加,最大拉伸载荷呈现先增大后减小的趋势,在体积掺入量为40 vol%时达到最大值。环氧树脂基体离纤维越近,对界面螯合效果的影响越大,其中有效界面厚度为纤维半径的0.128倍。纯环氧树脂-单纤维键合相的吸能为138.45 MJ/m3,而混合铝颗粒时环氧基与钨纤维有效键合面积的吸能为76.52 ~ 224.95 MJ/m3。
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来源期刊
Composites Science and Technology
Composites Science and Technology 工程技术-材料科学:复合
CiteScore
16.20
自引率
9.90%
发文量
611
审稿时长
33 days
期刊介绍: Composites Science and Technology publishes refereed original articles on the fundamental and applied science of engineering composites. The focus of this journal is on polymeric matrix composites with reinforcements/fillers ranging from nano- to macro-scale. CSTE encourages manuscripts reporting unique, innovative contributions to the physics, chemistry, materials science and applied mechanics aspects of advanced composites. Besides traditional fiber reinforced composites, novel composites with significant potential for engineering applications are encouraged.
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