Experimental study on water/CO2 flow of tight oil using HTHP microscopic visualization and NMR technology

IF 4.6 0 ENERGY & FUELS Geoenergy Science and Engineering Pub Date : 2025-07-01 Epub Date: 2025-03-12 DOI:10.1016/j.geoen.2025.213834
Jitian Ren , Wenlian Xiao , Qianrui Cheng , Peng Song , Xingyu Bai , Qichao Xie , Wanfen Pu , Lingli Zheng
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Abstract

The visualization of the transport and distribution of multiphase fluids through images is essential for understanding the mechanisms involved in the utilization of crude oil. In this study, we employed microscopic visualization and nuclear magnetic resonance technologies to monitor oil distribution and investigate fluid flow during water and supercritical CO2 flooding of tight core. The microscopic visualization experiment results indicate that during water flooding, significant viscous fingering occurred due to capillary pressure and an unfavorable mobility ratio, resulting in substantial volumes of contiguous residual oil and blind-end residual oil. In contrast, CO2 miscible flooding operates through interdependent interactions, facilitating the efficient extraction and displacement of residual oil, with an oil recovery of 93 % and a reduction in residual oil saturation of approximately 30 %. The NMR results demonstrate that the oil recovery of water flooding oil is 28.06 %, which is considerably lower than that of CO2 flooding, and the crude oil primarily comes from the macropores. We observed that the oil recovery of CO2 immiscible flooding, near-miscible flooding and miscible flooding yielded 41.35 %, 59.3 % and 66.22 %, respectively. The interaction between oil and CO2 resulted in a significant increase in oil recovery of macropores, approximately double that of immiscible flooding. As increasing injection pressure of CO2 flooding, the flow characteristics transition from capillary finger flow to a network flow, reducing residual oil saturation. This transition transforms significant volumes of contiguous residual oil into isolated oil droplets and smaller fragments, while alterations in water distribution characteristics influence CO2 flow. These findings provide valuable insights for optimizing displacement mechanisms and enhancing oil recovery in tight oil.
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高温高压显微可视化与核磁共振技术在致密油水/CO2流动中的实验研究
通过图像可视化多相流体的运移和分布对于理解原油利用的机制是必不可少的。本研究采用微观可视化和核磁共振技术监测致密岩心水驱和超临界CO2驱油过程中的油分布和流体流动情况。微观可视化实验结果表明,在水驱过程中,由于毛管压力和不利的流度比,产生了明显的粘指现象,导致大量的连续剩余油和盲端剩余油。相比之下,CO2混相驱通过相互依赖的相互作用进行操作,促进了剩余油的有效提取和驱替,原油采收率达到93%,剩余油饱和度降低了约30%。核磁共振结果表明,水驱油采收率为28.06%,明显低于CO2驱油采收率,原油主要来自大孔隙。结果表明,CO2非混相驱、近混相驱和混相驱的采收率分别为41.35%、59.3%和66.22%。油与CO2的相互作用使大孔隙的采收率显著提高,约为非混相驱的两倍。随着注入压力的增加,CO2驱的流动特征由毛细管指状流动转变为网状流动,残余油饱和度降低。这种转变将大量相邻的剩余油转化为孤立的油滴和更小的碎片,而水分布特征的变化影响了二氧化碳的流动。这些发现为优化致密油驱替机制和提高采收率提供了有价值的见解。
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