Influence of hot deformation process and annealing treatment on the microstructure of TC21 titanium alloy

IF 5.8 2区 材料科学 Q2 CHEMISTRY, PHYSICAL Journal of Alloys and Compounds Pub Date : 2025-03-21 DOI:10.1016/j.jallcom.2025.179939
Yang Xiang, Hengjun Luo, Wei Xiang, Qiang Fu, Wuhua Yuan
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Abstract

The TC21 alloy was subjected to hot compression tests at different strain rates (0.001 s-1~10 s-1), temperatures (890°C~1040°C), and deformation amount (0%~80%), followed by annealing at 900°C/1 h+AC. The microstructures of the samples were analyzed using OM, SEM, and EBSD techniques, and a systematic study of the microstructure evolution and flow softening mechanism was carried out, as well as an analysis of the variant selection phenomenon for the precipitation of α phase. The results show that the recrystallization mechanism of β grains in β region during deformation gradually changes from CDRX to DDRX with increasing strain rate and temperature; DRV is the dominant factor of the flow softening in the majority of deformation processes, which often occupies more than 50% of the contribution, and the contributions of deformation heat in α+β region and DRX in β region to flow softening cannot be neglected. The precipitated α phase will show the phenomenon of variant selection during the hot treatment in both α+β and β region, and the degree of variant selection decreases firstly and then rises as the deformation quantity increases, while it gradually decreases with the increase in temperature.
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在不同应变速率(0.001 s-1~10 s-1)、温度(890°C~1040°C)和变形量(0%~80%)下对 TC21 合金进行热压缩试验,然后在 900°C/1 h+AC 下进行退火。利用 OM、SEM 和 EBSD 技术分析了样品的微观结构,系统研究了微观结构演变和流动软化机理,并分析了 α 相析出的变体选择现象。结果表明,随着应变速率和温度的升高,β区β晶粒在变形过程中的再结晶机理由CDRX逐渐转变为DDRX;在大多数变形过程中,DRV是流动软化的主导因素,其贡献率往往超过50%,而且α+β区的变形热和β区的DRX对流动软化的贡献也不容忽视。在热处理过程中,析出的 α 相在 α+β 和 β 区都会出现变异选择现象,变异选择程度随着变形量的增加先减小后增大,而随着温度的升高则逐渐减小。
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来源期刊
Journal of Alloys and Compounds
Journal of Alloys and Compounds 工程技术-材料科学:综合
CiteScore
11.10
自引率
14.50%
发文量
5146
审稿时长
67 days
期刊介绍: The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.
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