Microstructure and mechanical properties of Ti-6Al-4V alloy fabricated using powder bed fusion – laser beam additive manufacturing process: Effect of hot isostatic pressing

IF 7 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Science and Engineering: A Pub Date : 2025-03-17 DOI:10.1016/j.msea.2025.148226
Linda Squillaci , Magnus Neikter , Thomas Hansson , Robert Pederson , Johan Moverare
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Abstract

Powder bed fusion laser beam (PBF-LB) is one of the most widespread and highly researched additive manufacturing (AM) methods, spanning multiple industries. Its feedstock material is metallic powder, where a conventional particle size range is 15–50 μm. The present study focuses on Ti-6Al-4V powder with a wider particle size distribution (15–90 μm). Two process themes are evaluated: one minimising porosity and one maximising build rate through a fast laser scanning speed. The effect of two hot isostatic pressing (HIP) heat treatments on mechanical properties, one below and one above the β-transus, are compared to those of as-built and stress relieved material. Room temperature impact toughness and tensile testing are used to compare the materials by determining UTS and Yield strength, elongation and reduction of area for the different process conditions and post build heat treatments. The minimal porosity theme reaches properties comparable to conventional manufacturing processes at all heat treatment temperatures (i.e., UTS >860 MPa, 0.2 % Yield >795 MPa). The high productivity theme treated below β-transus provides further improvement in overall reduction of area (>45 %) and elongation (>20 %) with respect to the minimal porosity theme, by showing a bi-modal microstructure that is the result of a recrystallisation process. This phenomenon is triggered by the closure of lack of fusion (LoF) defects via hot isostatic pressing, due to a higher dislocation density at the tip of these particular defects. Impact energy for this condition increases whilst hardness and texture become less pronounced. It is demonstrated that in those cases where a fast scanning speed creates LoF defects, those can assist in modifying microstructure during the consolidation process which has a positive effect on ductility.
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粉末床熔合-激光束增材制造Ti-6Al-4V合金的显微组织和力学性能:热等静压的影响
粉末床融合激光束(PBF-LB)是应用最广泛、研究最多的增材制造(AM)方法之一,涉及多个行业。其原料为金属粉末,常规粒度范围为15 ~ 50 μm。本文主要研究粒径分布较宽(15 ~ 90 μm)的Ti-6Al-4V粉末。评估了两个工艺主题:一个是通过快速激光扫描速度最小化孔隙率,一个是最大化构建速率。比较了两种热等静压(HIP)热处理对β-横截面以下和上方材料力学性能的影响。室温冲击韧性和拉伸测试用于比较材料,通过确定不同工艺条件和后期热处理的UTS和屈服强度,伸长率和面积收缩率。在所有热处理温度下(即UTS >;860 MPa, 0.2% Yield >795 MPa),最小孔隙率主题达到与传统制造工艺相当的性能。在β-横截面以下处理的高生产率主题,通过显示再结晶过程的双模态微观结构,相对于最小孔隙率主题,进一步提高了总体面积收缩率(> 45%)和伸长率(> 20%)。这种现象是由于在这些特殊缺陷的尖端有较高的位错密度,通过热等静压闭合缺乏熔合(LoF)缺陷而引发的。在这种情况下,冲击能量增加,而硬度和纹理变得不那么明显。结果表明,在产生LoF缺陷的情况下,快速扫描速度有助于改变固结过程中的微观结构,从而对延性产生积极影响。
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来源期刊
Materials Science and Engineering: A
Materials Science and Engineering: A 工程技术-材料科学:综合
CiteScore
11.50
自引率
15.60%
发文量
1811
审稿时长
31 days
期刊介绍: Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.
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