High-temperature fatigue cracking mechanism and microstructure evolution of aero-engine K4169 superalloy in service process

IF 4.7 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Transactions of Nonferrous Metals Society of China Pub Date : 2025-02-01 Epub Date: 2025-03-22 DOI:10.1016/S1003-6326(24)66695-1
Song-jun WANG , Jian-jun HE , Zhi-hui GONG , Wei-ping LI , Jun-gang YANG , Ya-jun SHAO , Yu-hui CAI , Yue-xin DU , Cheng-wei YANG
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Abstract

By using fatigue crack propagation testing and microstructural characterization, the crack fracture and propagation mechanisms of K4169 superalloy under various loads were investigated. The results demonstrate that the grain sizes of K4169 superalloy significantly increase, and the precipitation of the needle-like δ phase and the Laves phase is observed. Voids and microcracks form at location of Laves phase enrichment, creating conditions for crack propagation. By the aN (a is the crack length, and N is the number of cycles) relationship curve, the change in the fatigue crack growth rate with the increasing number of cycles progresses through three separate stages. The fracture process of K4169 superalloy under low-stress cyclic loading (3 kN) exhibits the ductile fracture. Subsequently, the fracture process starts to change from the ductile fracture to the brittle fracture as the stress increases to 4.5 kN. In the microstructures of fractures in both stress states, intergranular propagation is the mechanism responsible for crack propagation. Moreover, the Laves phase exists near the fracture crack, which is in line with the post-service structural phenomenon.
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航空发动机K4169高温合金服役过程高温疲劳开裂机理及组织演变
通过疲劳裂纹扩展测试和微结构表征,研究了 K4169 超合金在各种载荷下的裂纹断裂和扩展机理。结果表明,K4169 超耐热合金的晶粒尺寸明显增大,出现了针状 δ 相和 Laves 相的析出。在 Laves 相富集的位置形成了空隙和微裂纹,为裂纹扩展创造了条件。根据 a-N(a 为裂纹长度,N 为循环次数)关系曲线,随着循环次数的增加,疲劳裂纹增长率的变化经历了三个不同的阶段。K4169 超级合金在低应力循环加载(3 kN)下的断裂过程表现为韧性断裂。随后,当应力增加到 4.5 kN 时,断裂过程开始从韧性断裂转变为脆性断裂。在这两种应力状态下的断口微观结构中,晶间扩展是裂纹扩展的主要机制。此外,在断裂裂纹附近存在 Laves 相,这与使用后的结构现象一致。
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来源期刊
CiteScore
7.40
自引率
17.80%
发文量
8456
审稿时长
3.6 months
期刊介绍: The Transactions of Nonferrous Metals Society of China (Trans. Nonferrous Met. Soc. China), founded in 1991 and sponsored by The Nonferrous Metals Society of China, is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology, including mineral processing, extraction metallurgy, metallic materials and heat treatments, metal working, physical metallurgy, powder metallurgy, with the emphasis on fundamental science. It is the unique preeminent publication in English for scientists, engineers, under/post-graduates on the field of nonferrous metals industry. This journal is covered by many famous abstract/index systems and databases such as SCI Expanded, Ei Compendex Plus, INSPEC, CA, METADEX, AJ and JICST.
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