Study on the ceramic fused filament fabrication process and the built parts’ static mechanical properties

IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING International Journal of Material Forming Pub Date : 2025-03-26 DOI:10.1007/s12289-025-01892-w
Shijie Jiang, Hongwei Ying, Jiaqi Chen, Yuntao Zhang, Shanggang Cai, Shuo Liu
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Abstract

Ceramic fused filament fabrication (CF3), a type of ceramic additive manufacturing technology, uses ceramic powder/polymer composite filament as raw material to fabricate densified ceramic parts through shaping-debinding-sintering (S-D-S) process, and it owns broad application and development prospects. However, the existing study on the static mechanical properties of CF3 parts is still in the basic stage, lacking comprehensiveness and systematicity. In this paper, self-made zirconia/polymer composite filament with a five-component binder system was developed, and the ME equipment was used to shape the green specimens with different processing parameters (layer thickness, solid loading and infill angle) in order to verify the formability of the composite filament; They were then debinded and sintered using the box sintering furnace so as to obtain the sintered CF3 specimens; Finally, experimental studies on their physical and static properties were carried out to investigate the effects of processing parameters. The results showed that increasing the solid loading of zirconia significantly reduced the dimensional shrinkage of the sintered specimens; When the layer thickness increased from 0.2 to 0.3 mm, the compressive strength decreased from 358.66 to 213.40 MPa, and the bending strength decreased from 456.01 to 293.12 MPa; When the infill angle increased from 0° to 90°, the bending strength of the specimens decreased from 456.01 to 120.08 MPa; The Vickers hardness of the sintered specimens was independent, and it has the characteristic of isotropy.

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陶瓷熔丝的制备工艺及制品的静态力学性能研究
陶瓷熔丝制造(CF3)是一种陶瓷增材制造技术,以陶瓷粉末/聚合物复合长丝为原料,通过成型-脱脂-烧结(S-D-S)工艺制备致密化陶瓷零件,具有广阔的应用和发展前景。然而,目前对CF3零件静态力学性能的研究还处于基础阶段,缺乏全面性和系统性。本文研制了自制的五组分粘结剂体系氧化锆/聚合物复合长丝,并利用ME设备对不同工艺参数(层厚、固相载荷、填充角度)的绿色试样进行了成型,验证了复合长丝的成型性能;然后用箱式烧结炉对其进行脱脂和烧结,得到烧结后的CF3试样;最后,对其物理和静态性能进行了实验研究,探讨了加工参数对其性能的影响。结果表明:增加氧化锆的固体载荷可显著降低烧结试样的尺寸收缩率;当层厚从0.2 mm增加到0.3 mm时,抗压强度从358.66降低到213.40 MPa,抗弯强度从456.01降低到293.12 MPa;当充填角从0°增加到90°时,试件的抗弯强度从456.01降低到120.08 MPa;烧结试样的维氏硬度是独立的,具有各向同性的特点。
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来源期刊
International Journal of Material Forming
International Journal of Material Forming ENGINEERING, MANUFACTURING-MATERIALS SCIENCE, MULTIDISCIPLINARY
CiteScore
5.10
自引率
4.20%
发文量
76
审稿时长
>12 weeks
期刊介绍: The Journal publishes and disseminates original research in the field of material forming. The research should constitute major achievements in the understanding, modeling or simulation of material forming processes. In this respect ‘forming’ implies a deliberate deformation of material. The journal establishes a platform of communication between engineers and scientists, covering all forming processes, including sheet forming, bulk forming, powder forming, forming in near-melt conditions (injection moulding, thixoforming, film blowing etc.), micro-forming, hydro-forming, thermo-forming, incremental forming etc. Other manufacturing technologies like machining and cutting can be included if the focus of the work is on plastic deformations. All materials (metals, ceramics, polymers, composites, glass, wood, fibre reinforced materials, materials in food processing, biomaterials, nano-materials, shape memory alloys etc.) and approaches (micro-macro modelling, thermo-mechanical modelling, numerical simulation including new and advanced numerical strategies, experimental analysis, inverse analysis, model identification, optimization, design and control of forming tools and machines, wear and friction, mechanical behavior and formability of materials etc.) are concerned.
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