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A comparative study of conformal and traditional cooling system for optimizing molding time and warpage reduction 优化成型时间和减少翘曲的保形冷却系统与传统冷却系统的比较研究
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-20 DOI: 10.1007/s12289-026-01979-y
Junhui Liu, Liping Luo, Xiaojie Feng, Junwu Luo

In the injection molding process, cooling efficiency and uniformity significantly influence product quality and cycle time. This paper presents a multi-objective optimization study aiming to minimize both molding time and maximum warpage through process parameter tuning, while comparing the performance of traditional and conformal cooling systems. Using Latin Hypercube Sampling, 15 process parameter sets were simulated in Moldflow. A radial basis function neural network was trained to model the relationship between process parameters and quality objectives, followed by particle swarm optimization to obtain Pareto fronts for both cooling systems. Experimental validation confirmed simulation accuracy with errors below 5%. The results show that through optimized process parameters, conformal cooling achieved a trade-off between warpage and molding time in the ranges of approximately 0.25 ~ 0.51 mm and 12.9 ~ 15.8 s, respectively. Compared to traditional cooling, the conformal system reduced maximum warpage by about 25% and molding time by 30% on average, thereby shortening the molding cycle and improving efficiency while enhancing product quality.

在注射成型过程中,冷却效率和均匀性对产品质量和循环时间有重要影响。本文提出了一种多目标优化研究,旨在通过工艺参数调整最小化成型时间和最大翘曲,同时比较了传统冷却系统和保形冷却系统的性能。采用拉丁超立方体采样,在Moldflow中模拟了15个工艺参数集。采用径向基函数神经网络对工艺参数与质量目标之间的关系进行建模,并采用粒子群算法求解两种冷却系统的Pareto前沿。实验验证了仿真精度,误差在5%以下。结果表明,通过优化工艺参数,保形冷却使翘曲时间和成型时间分别在0.25 ~ 0.51 mm和12.9 ~ 15.8 s之间实现了平衡。与传统的冷却方式相比,保形系统的最大翘曲量平均减少了25%左右,成型时间平均减少了30%,从而缩短了成型周期,提高了效率,同时提高了产品质量。
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引用次数: 0
Topological construction of forming geometry features for complex sheet metal parts 复杂钣金件成形几何特征的拓扑构造
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-19 DOI: 10.1007/s12289-025-01966-9
Gui Li, Zhijie Tan, Yaodong Liu, Tianyu Li

Complex sheet metal parts are manufactured through multi-stage plastic deformation processes. The geometric configuration design, feature recognition, and segmentation of these forming stages constitute a core challenge in intelligent die design. This demands systematic planning integrating material behavior, process constraints, and tool structure, thus necessitating precise geometric understanding of the part. To address this, we propose a spectral-graph-theory-based approach for analyzing forming-feature attributes. A topological model of geometric features is established to support optimal forming-stage geometry design. Beginning with the 3D surface model, elementary geometric features are extracted, and their mean curvatures are adopted as primary graph signals. A weighted Laplacian matrix is constructed using Gaussian kernel weights, with its eigen decomposition yielding the spectral graph representation of the part. Spectral clustering then partitions this graph into distinct subgraphs, each corresponding to an individual geometric forming feature. This facilitates the establishment of a topological structure graph for forming features, enabling robust feature recognition. Validation via recognition and design case studies demonstrate that the method efficiently translates geometric features into frequency-domain signals through mathematical modeling. This achieves effective feature extraction and classification, confirming its significant potential for advancing process design and manufacturing in sheet-metal forming.

复杂的钣金件是通过多阶段的塑性变形过程制造出来的。这些成形阶段的几何形态设计、特征识别和分割是智能模具设计的核心挑战。这就要求系统地规划材料性能、工艺约束和工具结构,从而需要对零件进行精确的几何理解。为了解决这个问题,我们提出了一种基于谱图理论的方法来分析形成特征属性。建立了几何特征的拓扑模型,以支持成形阶段的最优几何设计。从三维曲面模型入手,提取初等几何特征,取其平均曲率作为初等图形信号。利用高斯核权构造加权拉普拉斯矩阵,其特征分解得到部件的谱图表示。然后,谱聚类将该图划分为不同的子图,每个子图对应一个单独的几何形状特征。这有助于建立拓扑结构图,形成特征,实现鲁棒特征识别。通过识别和设计实例的验证表明,该方法通过数学建模有效地将几何特征转换为频域信号。这实现了有效的特征提取和分类,证实了其在推进钣金成形工艺设计和制造方面的巨大潜力。
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引用次数: 0
Influence of initial deformation on microstructural and textural evolution of pure copper under severe plastic deformation 初始变形对纯铜在剧烈塑性变形下组织演变的影响
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-19 DOI: 10.1007/s12289-026-01976-1
Muhammad Rifai, Mujamilah Mujamilah, Grace Tj Sulungbudi, Andon Insani, Ahadi Damar Prasetya, Emy Mulyani, Taufik Taufik

This study reveals the fundamental microstructural and textural transformations that occur in high-purity copper after a single pass of Equal Channel Angular Pressing (ECAP). The main issue addressed is the lack of understanding regarding the onset of grain refinement and texture development during the early stage of severe plastic deformation (SPD) in face-centered cubic (FCC) metals. Contrary to the common focus on multi-pass processing, this work demonstrates that even a single ECAP pass induces significant microstructural reorganization. Transmission Electron Microscopy (TEM) and Electron Backscatter Diffraction (EBSD) analyses show the formation of dense dislocation networks, subgrains, and a notable increase in high-angle grain boundaries (HAGBs), indicating the transition from a coarse-grained to an ultrafine-grained (UFG) structure. X-ray diffraction pole figure analysis reveals a pronounced shear texture characterized by {111}<110 > and {112}<110 > components. These findings highlight that substantial structural and crystallographic changes can be initiated through minimal deformation. The innovation of this work lies in its demonstration that meaningful grain refinement and texture evolution begin at the very first stage of ECAP, offering valuable insights for designing SPD strategies to tailor material properties. This contribution forms a critical basis for optimizing ECAP-based processing routes in copper and similar FCC metals, even at the initial deformation step.

本研究揭示了高纯铜在经过一次等通道角压(ECAP)后发生的基本微观结构和织构转变。研究的主要问题是缺乏对面心立方(FCC)金属严重塑性变形(SPD)早期阶段晶粒细化和织构发展的理解。与通常关注的多道次处理相反,这项工作表明,即使是单一的ECAP经过也会引起显著的微观结构重组。透射电子显微镜(TEM)和电子背散射衍射(EBSD)分析表明,该材料形成了密集的位错网络和亚晶,高角度晶界(HAGBs)明显增加,表明其由粗晶向超细晶(UFG)结构转变。x射线衍射极图分析显示具有明显的剪切结构,其特征为{111}<;110 >;和{112}<;110 >;分量。这些发现强调,通过最小的变形可以引发实质性的结构和晶体学变化。这项工作的创新之处在于它证明了有意义的晶粒细化和纹理演变始于ECAP的第一阶段,为设计SPD策略以定制材料性能提供了有价值的见解。这一贡献为优化铜和类似FCC金属的ecap加工路线奠定了关键基础,即使在初始变形步骤也是如此。
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引用次数: 0
Hot Forging-Based development of mining drill bit preforms: experimental and numerical analysis 基于热锻的矿用钻头预制件研制:试验与数值分析
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-16 DOI: 10.1007/s12289-026-01975-2
Charles Chemale Yurgel, Nick M. Rockwell, Wojciech Z. Misiolek, Fábio A. Lora, Ricardo Alves de Sousa

Low-alloy steel drill bits are commonly used in the mining industry for boring holes into rocks. They are characterized by high hardenability and a good combination of mechanical properties, with minimal additions of alloying elements. As product quality improves, the market becomes more competitive. Significant growth in the use of engineering development tools has also occurred, leading to improved performance in rock drilling, oil and mineral exploration, and the search for gemstones. Due to the constant cyclical mechanical stresses applied, the expected life of drill bits is often reduced by fatigue or mechanical wear, indicating that the market consistently requires the availability of new drill bits. This work aimed to demonstrate the suitability of hot forging as a substitute for machining to manufacture the specific profile of the drill bit preform used in rock drilling. A mining-industry partner selected AISI 8640 steel, as it is widely used for drilling applications. Tests were performed with AISI 8640 as a modeling material, and the results from the forging process were used to evaluate the punch movement and consequent metal flow, as well as the filling of the part’s cavity within the forging dies. The results obtained using Elementary Plasticity Theory (EPT) allowed verification of the physical experiment with AISI 8640 steel forged parts. Following this evaluation, numerical modeling was performed and compared with the hot forging process. Formation of the hollow cavity(sigma_b) within the part and the head of the preform in the same step was assessed. As a result of this optimized process, the reduction in the initial height of the billet and the preform formation were analyzed, with the finishing of the drill bit contingent upon the machining process. This hot forging demonstrated improved material utilization compared to the machining process, highlighting the benefits of deformation through simulations.

低合金钢钻头在采矿业中通常用于在岩石上钻孔。它们的特点是高淬透性和良好的综合机械性能,添加的合金元素很少。随着产品质量的提高,市场竞争日趋激烈。工程开发工具的使用也出现了显著增长,从而提高了岩石钻探、石油和矿产勘探以及寻找宝石的性能。由于不断施加周期性的机械应力,钻头的预期寿命通常会因疲劳或机械磨损而降低,这表明市场一直需要新的钻头。这项工作的目的是证明热锻造作为机械加工的替代品的适用性,以制造用于岩石钻探的钻头预制件的特定轮廓。一家采矿业合作伙伴选择了AISI 8640钢材,因为它广泛用于钻井应用。以AISI 8640为建模材料进行了试验,并使用锻造过程的结果来评估冲头运动和随之而来的金属流动,以及锻模内零件腔的填充。利用初等塑性理论(EPT)对aisi8640钢锻件的物理实验结果进行了验证。在此基础上,进行了数值模拟,并与热锻过程进行了比较。在同一步骤中评估了零件和预制件头部内形成的空心腔(sigma_b)。通过优化后的工艺,分析了坯料初始高度和预成形的降低情况,并对钻头的精加工工艺进行了分析。与机械加工工艺相比,这种热锻工艺证明了材料利用率的提高,通过模拟突出了变形的好处。
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引用次数: 0
Coupled process chain modelling to minimise the earing formation in industrially rolled aluminium strips for beverage can production using data-based methods 耦合过程链建模,以尽量减少耳形成工业轧制铝带饮料罐生产使用基于数据的方法
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-13 DOI: 10.1007/s12289-025-01972-x
Nilesh Thakare, Kai Karhausen, Hans-Reimund Müller, Emad Scharifi, David Bailly

The production of aluminium strip involves a long sequence of thermomechanical processing steps that significantly influence the material’s mechanical properties and may induce anisotropy. This anisotropy can manifest as earing during deep drawing operations - such as those used in beverage can manufacturing - resulting in increased trimming scrap, process downtimes, and reduced economic viability. To assess formability and quantify earing, the cup drawing test is employed as a standard evaluation method. Understanding and minimizing earing formation requires comprehensive modelling of the entire process chain, which is traditionally performed manually by domain experts - a time-consuming, error-prone, and costly effort. This study presents a novel, scalable, and flexible approach to model a process chain by integrating production data with process models on the Microsoft Azure Databricks platform. The proposed method is validated on an industrial aluminium strip production line, demonstrating its capability to automate data processing, extract actionable insights, and support process optimisation. The approach successfully identifies an optimum processing route that minimises the earing integral, as determined by a dedicated evaluation function.

铝带的生产涉及一系列的热机械加工步骤,这些步骤对材料的机械性能有很大的影响,并可能导致各向异性。这种各向异性可以表现为在深拉深操作中的磨损-例如在饮料罐制造中使用的那些-导致切边废料增加,工艺停机时间和经济可行性降低。为了评估成形性和量化成形,采用杯形拉伸试验作为标准评价方法。理解和最小化收益形成需要对整个流程链进行全面建模,传统上这是由领域专家手动执行的,这是一项耗时、容易出错且代价高昂的工作。本研究提出了一种新颖的、可扩展的、灵活的方法,通过将生产数据与Microsoft Azure Databricks平台上的流程模型集成来建模流程链。该方法在一条工业铝带生产线上进行了验证,证明了其自动化数据处理、提取可操作见解和支持流程优化的能力。该方法成功地确定了一个最佳的处理路线,使耳积分最小化,由一个专门的评估函数确定。
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引用次数: 0
Effect of energy density on the forming quality of 6063 aluminum alloy fabricated by selective laser melting 能量密度对选择性激光熔化6063铝合金成形质量的影响
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-13 DOI: 10.1007/s12289-025-01974-9
Xutao You, Fenggang G. Liu, Fencheng Liu, Jiaying Gao, Xin Wang, Menglan Tang, Chunping P. Huang, Qiuge Li

This paper studied the effect of energy density on the formability of the selective laser melting (SLM) 6063 aluminum alloy, and analyzed the density, surface quality, microstructure and mechanical property. In the SLM 6063 aluminum alloy, there were mainly two kinds of pore defects, i.e. non-fusion and pores. When the energy density was low (< 100 J/mm3), serious solidification crack defects existed in the specimen. With the increase of energy density, the crack defects in the specimen gradually improved. At the same time, the density generally showed a trend of first increasing and then decreasing. The energy density range of 66.67 ~ 100 J/mm3 was more conducive to the forming of high-density specimens (> 97%). The microhardness of the SLM 6063 aluminum alloy in each group was about 40 HV, which was less affected by process parameters. When the scanning speed was constant, with the increase of laser power, the tensile strength of the specimen first increased and then decreased, and the elongation first decreased and then increased. When the laser power was constant, the tensile strength of the specimen decreased sharply with the increase of scanning speed, and the elongation increased first and then decreased. Considering the density, crack defects and mechanical properties of the specimens under different process parameters, the laser power of 360 W, the scanning speed of 1000 mm/s, and the scanning spacing of 0.1 mm were identified as optimal process parameters, which can be used as a theoretical reference for the preparation of high-quality SLM aluminum alloy.

研究了能量密度对选择性激光熔化(SLM) 6063铝合金成形性能的影响,分析了能量密度、表面质量、显微组织和力学性能。在SLM 6063铝合金中,主要存在两种孔隙缺陷,即未熔合缺陷和气孔缺陷。当能量密度较低(< 100 J/mm3)时,试样存在严重的凝固裂纹缺陷。随着能量密度的增加,试样中的裂纹缺陷逐渐改善。同时,密度总体上呈现先增大后减小的趋势。能量密度在66.67 ~ 100 J/mm3范围内更有利于高密度试样的形成(> 97%)。各组SLM 6063铝合金的显微硬度均在40 HV左右,受工艺参数的影响较小。当扫描速度一定时,随着激光功率的增大,试样的抗拉强度先增大后减小,伸长率先减小后增大。当激光功率一定时,试样的抗拉强度随扫描速度的增加而急剧下降,伸长率先增大后减小。综合考虑不同工艺参数下试样的密度、裂纹缺陷和力学性能,确定了激光功率为360 W、扫描速度为1000 mm/s、扫描间距为0.1 mm为最佳工艺参数,可为制备高质量的SLM铝合金提供理论参考。
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引用次数: 0
Research on springback prediction of S600 aluminum alloy sheets based on in-plane anisotropy and hybrid strengthening model 基于面内各向异性和混合强化模型的S600铝合金板回弹预测研究
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-01-09 DOI: 10.1007/s12289-025-01973-w
Zhuoyun Yang, Jinjin Wang, Yuyang Fang, Hanpeng Yu, Guojiang Dong

Aluminum alloy sheets are widely used in lightweight industries due to their excellent performance, but the springback defects in complex forming processes are difficult to predict and control precisely. In this paper, S600 high-strength aluminum was taken as the target. A method combining theoretical analysis, finite element simulation, and forming-process tests was adopted to develop the model. The multi-objective improved non-dominated sorting genetic algorithm was used to optimize the anisotropic yield criterion parameters of Yld2000-2D anisotropic yield criterion. Subsequently, a hybrid calibration strategy combining the multi-objective optimization algorithm and the inverse solution method was adopted to collaboratively optimize the parameters of the Chaboche hybrid strengthening model. And the springback simulation and forming test were conducted to verify the accuracy of springback prediction of the established constitutive models. For two-dimensional cylindrical surface and three-dimensional space complex surface, the maximum prediction deviations of the Yld2000-2D-Chaboche model have increased 24.3% and 12.7% respectively. For different stamping amounts (20 mm and 30 mm) of the C-shaped beam, the average errors were 0.2 mm and 0.06 mm respectively. This series of comparative verifications not only confirmed the accuracy of the optimized Yld2000-2D-Chaboche model, but also fully proved its wide applicability in complex forming processes.

铝合金薄板以其优异的性能在轻量化工业中得到广泛应用,但复杂成形过程中的回弹缺陷难以精确预测和控制。本文以S600高强铝为研究对象。采用理论分析、有限元模拟和成形过程试验相结合的方法建立了该模型。采用多目标改进非支配排序遗传算法对Yld2000-2D各向异性产量准则参数进行优化。随后,采用多目标优化算法和逆解法相结合的混合标定策略,对Chaboche混合强化模型的参数进行协同优化。并进行了回弹模拟和成形试验,验证了所建立的本构模型回弹预测的准确性。对于二维圆柱面和三维空间复杂面,Yld2000-2D-Chaboche模型的最大预测偏差分别提高了24.3%和12.7%。对于不同冲压量(20 mm和30 mm)的c形梁,平均误差分别为0.2 mm和0.06 mm。这一系列的对比验证不仅证实了优化后的Yld2000-2D-Chaboche模型的准确性,也充分证明了其在复杂成形过程中的广泛适用性。
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引用次数: 0
Characterisation and modelling of ductile fracture in incremental sheet forming of an aluminium alloy with consideration of temperature variations 考虑温度变化的铝合金薄板渐进成形韧性断裂的表征与建模
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2025-12-26 DOI: 10.1007/s12289-025-01970-z
Zhenyuan Qin, Shakir Gatea, Hengan Ou

Although extensive studies have been conducted to predict ductile fracture at room temperature, no attempt has been made to use Gurson–Tvergaard–Needleman (GTN) model to capture the effect of temperature due to spindle speed induced friction heat on damage accumulation in incremental sheet forming (ISF). In this work, the temperature effect is incorporated into a shear modified GTN model to characterise ductile fracture behaviour of an aluminium alloy (AA1050) at varying temperatures in ISF processing under different strain states. The correlation between void evolution and damage accumulation at different temperatures is revealed, and the void volume fraction (VVF) at different deformation stages is determined by conducting microscopic in-situ tensile test. By introducing a new temperature-dependent VVF function and determining appropriate GTN damage parameters, ductile fracture under different ISF processing temperatures is evaluated using FE simulation and validated by ISF experimental testing. The results show that the proposed temperature-dependent VVF function in GTN modelling is capable of predicting the ductile fracture of both the set temperatures in in-situ tensile tests and the varying temperature conditions in ISF processes. This study unveils the underlying mechanisms behind material deformation and damage evolution with consideration of temperature variations caused by tool spindle speed at various ISF forming conditions, which provides guidance for process optimisation and formability improvement in ISF process.

虽然已经进行了大量的研究来预测室温下的韧性断裂,但还没有尝试使用Gurson-Tvergaard-Needleman (GTN)模型来捕捉由于主轴速度引起的摩擦热对增量板成形(ISF)中损伤积累的影响。在这项工作中,将温度效应纳入剪切修正GTN模型,以表征不同应变状态下ISF加工中铝合金(AA1050)在不同温度下的韧性断裂行为。揭示了不同温度下孔隙演化与损伤积累的相关性,并通过显微原位拉伸试验确定了不同变形阶段的孔隙体积分数(VVF)。通过引入新的温度相关VVF函数,确定合适的GTN损伤参数,采用有限元模拟方法评估了不同ISF处理温度下的韧性断裂,并通过ISF实验测试进行了验证。结果表明,GTN模型中提出的温度相关VVF函数能够预测原位拉伸试验设定温度和ISF过程变温度条件下的韧性断裂。该研究揭示了在不同ISF成形条件下,考虑刀具主轴转速引起的温度变化的材料变形和损伤演变的潜在机制,为ISF工艺优化和成形性改善提供了指导。
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引用次数: 0
A novel approach for fabricating tubes with variable wall thicknesses in hollow sinking 一种制造变壁厚空心沉管的新方法
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2025-12-22 DOI: 10.1007/s12289-025-01971-y
Takuma Kishimoto, Hisashi Sato

Variable wall-thickness tubes are increasingly required for lightweight, functionally optimized structures and heat-transfer components, yet conventional hollow sinking with a constant speed ratio between the feeding and drawing sides produces an almost uniform wall thickness along the tube axis and cannot generate a taper. This study proposes a simple hollow sinking process for fabricating variable wall-thickness microtubes without an inner tool by controlling the speed ratio between the feeding and drawing sides, that is, by increasing the drawing speed during processing while keeping the feeding speed at the die entrance constant. Austenitic stainless-steel (SUS304) tubes with an outer diameter of 2.0 mm, an inner diameter of 1.82 mm, and an initial wall thickness of 0.09 mm were drawn under these conditions, where the drawing speed on the exit side was continuously increased while the feeding speed was fixed. The resulting wall-thickness distributions and surface roughness were evaluated experimentally and by finite-element analysis, which consistently showed that the increasing speed ratio enhances the axial elongation per unit time beneath and just after the die, thereby geometrically introducing a taper slope on the inner wall. Using this method, tubes with a maximum wall-thickness difference of about 40% between thick and thin sections were fabricated while maintaining acceptable outer and inner surface quality. These results demonstrate that variable-thickness microtubes can be intentionally produced in hollow sinking through simple control of the speed ratio between the feeding and drawing sides, extending the conventional geometric framework for straight tubes to tapered tubes.

变壁厚管越来越需要轻量化、功能优化的结构和传热组件,然而传统的空心沉管在进料和拉拔侧之间具有恒定的速比,沿管轴产生几乎均匀的壁厚,并且不能产生锥度。本研究提出了一种简单的无内刀制变壁厚微管的空心开孔工艺,通过控制进、拉边速比,即在加工过程中提高拉边速度,同时保持模具入口的进给速度不变。在此条件下,拉拔外径为2.0 mm,内径为1.82 mm,初始壁厚为0.09 mm的奥氏体不锈钢(SUS304)管,在固定进给速度的情况下,不断提高出口侧拉拔速度。通过实验和有限元分析对得到的壁厚分布和表面粗糙度进行了评估,结果一致表明,速比的增加提高了模下和模后单位时间的轴向伸长率,从而在几何上在内壁上引入了锥度斜率。使用这种方法,可以在保持可接受的外表面和内表面质量的同时,制造出厚和薄截面之间最大壁厚差约40%的管。这些结果表明,通过简单控制进料边和拉深边之间的速比,将传统的直管几何框架扩展到锥形管,可以在空心凹槽中有意地生产变厚度微管。
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引用次数: 0
Influence of extrusion and ECAP processes on mechanical, tribological and corrosion properties of biodegradable Zn1AgCuMg alloy 挤压和ECAP工艺对可生物降解Zn1AgCuMg合金力学、摩擦学和腐蚀性能的影响
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2025-12-19 DOI: 10.1007/s12289-025-01969-6
Sinan Sezek, Bunyamin Aksakal

Zn-based alloys have attracted significant attention as potential candidates for biodegradable implants due to their excellent biocompatibility; however, their inherently low tribological performance continues to restrict practical applications. In the present study, a Zn1AgCuMg alloy was fabricated via induction melting–casting and subsequently processed through cold extrusion and equal channel angular pressing (ECAP) using various routes (A, C, R, Bc) and pass numbers (1–4). The processing resulted in substantial microstructural refinement, reducing the average grain size from 245 μm in the as-cast condition to 72 μm after ECAP Route-Bc with four passes, accompanied by an increase in hardness from 62 HV to 113 HV. The yield strength improved from 150 MPa (as-cast) to 164 MPa after extrusion, and further to 217 MPa following ECAP Route-Bc (four passes). Similarly, the corrosion rate decreased from 294 mpy in the untreated alloy to 232 mpy after extrusion and to 66.16 mpy after ECAP Route-Bc (four passes). Tribological assessment revealed negligible differences between extrusion and 1–2 pass ECAP samples; however, a marked enhancement in wear resistance was observed in the 3–4 pass ECAP conditions, with the lowest friction coefficient (0.083) achieved for ECAP Route-Bc (four passes). These results confirm that controlled severe plastic deformation via ECAP can concurrently improve mechanical strength, wear resistance, and corrosion resistance in Zn-based biodegradable alloys, with multi-pass ECAP Route-Bc offering the most balanced performance for prospective implant applications.

由于锌基合金具有良好的生物相容性,作为生物可降解植入物的潜在候选物受到了广泛的关注;然而,其固有的低摩擦学性能继续限制了实际应用。在本研究中,通过感应熔铸制备了Zn1AgCuMg合金,随后通过冷挤压和等道角压(ECAP),采用不同的路线(a, C, R, Bc)和孔道号(1-4)进行加工。经过四道次ECAP Route-Bc处理,合金的平均晶粒尺寸从铸态时的245 μm减小到72 μm,硬度从62 HV提高到113 HV。屈服强度由铸态时的150 MPa提高到挤压后的164 MPa,采用ECAP路线- bc(四道次)后的屈服强度进一步提高到217 MPa。同样,腐蚀速率从未处理合金的294 mpy下降到挤压后的232 mpy, ECAP Route-Bc(四道)后的66.16 mpy。摩擦学评估显示,挤压和1-2个通过ECAP样品之间的差异可以忽略不计;然而,在3-4次ECAP条件下,观察到耐磨性明显增强,ECAP Route-Bc(4次)的摩擦系数最低(0.083)。这些结果证实,通过ECAP控制的严重塑性变形可以同时提高锌基可生物降解合金的机械强度、耐磨性和耐腐蚀性,多道ECAP Route-Bc为未来的植入物应用提供了最平衡的性能。
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引用次数: 0
期刊
International Journal of Material Forming
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