Microwave-Assisted Facile Synthesis of 1,2-Benzisoxazoles, Isoxazoloquinolines, and Isothiazoloquinolines in [BMIM(SO2Cl)][OTs] Ionic Liquid as a Recyclable System

IF 0.8 4区 化学 Q4 CHEMISTRY, MULTIDISCIPLINARY Russian Journal of General Chemistry Pub Date : 2025-03-26 DOI:10.1134/S1070363224611943
I. Jamadar, R. B. Manami, S. Kurahatti, A. Anchi, V. Jadhav, R. G. Kalkhambkar, M. Kurkuri, M. S. Refat, A. M. Alsuhaibani
{"title":"Microwave-Assisted Facile Synthesis of 1,2-Benzisoxazoles, Isoxazoloquinolines, and Isothiazoloquinolines in [BMIM(SO2Cl)][OTs] Ionic Liquid as a Recyclable System","authors":"I. Jamadar,&nbsp;R. B. Manami,&nbsp;S. Kurahatti,&nbsp;A. Anchi,&nbsp;V. Jadhav,&nbsp;R. G. Kalkhambkar,&nbsp;M. Kurkuri,&nbsp;M. S. Refat,&nbsp;A. M. Alsuhaibani","doi":"10.1134/S1070363224611943","DOIUrl":null,"url":null,"abstract":"<p>A green method of the synthesis of 1,2-benzisoxazole, isoxazolo- and isothiazolo-quinoline from 2-hydroxyaryl ketoximes in the presence of [BMIM(SO<sub>2</sub>Cl)][OTs] ionic liquid has been demonstrated under microwave irradiation. The noticeable advantages of this method over other reported methods are less reaction time, simple work-up procedure and excellent yields (85–96%). The method also highlights the reuse and recycle of ionic liquid employed (up to four cycles) with negligible loss of yield.</p>","PeriodicalId":761,"journal":{"name":"Russian Journal of General Chemistry","volume":"95 2","pages":"393 - 404"},"PeriodicalIF":0.8000,"publicationDate":"2025-03-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of General Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S1070363224611943","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

Abstract

A green method of the synthesis of 1,2-benzisoxazole, isoxazolo- and isothiazolo-quinoline from 2-hydroxyaryl ketoximes in the presence of [BMIM(SO2Cl)][OTs] ionic liquid has been demonstrated under microwave irradiation. The noticeable advantages of this method over other reported methods are less reaction time, simple work-up procedure and excellent yields (85–96%). The method also highlights the reuse and recycle of ionic liquid employed (up to four cycles) with negligible loss of yield.

Abstract Image

查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
[BMIM(SO2Cl)][OTs]离子液体中微波辅助快速合成1,2-苯并异恶唑、异恶唑喹啉和异噻唑喹啉
研究了在[BMIM(SO2Cl)][OTs]离子液体存在下,微波辐射下由2-羟基酮肟合成1,2-苯并异恶唑、异恶唑和异噻唑喹啉的绿色方法。与其他已报道的方法相比,该方法的显著优点是反应时间短,工序简单,收率高(85-96%)。该方法还强调了离子液体的再利用和再循环(多达四个循环),而产量的损失可以忽略不计。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
CiteScore
1.40
自引率
22.20%
发文量
252
审稿时长
2-4 weeks
期刊介绍: Russian Journal of General Chemistry is a journal that covers many problems that are of general interest to the whole community of chemists. The journal is the successor to Russia’s first chemical journal, Zhurnal Russkogo Khimicheskogo Obshchestva (Journal of the Russian Chemical Society ) founded in 1869 to cover all aspects of chemistry. Now the journal is focused on the interdisciplinary areas of chemistry (organometallics, organometalloids, organoinorganic complexes, mechanochemistry, nanochemistry, etc.), new achievements and long-term results in the field. The journal publishes reviews, current scientific papers, letters to the editor, and discussion papers.
期刊最新文献
Enhancing Hydrophobicity of Organic Membranes via Petroleum Resin and Nanoparticle Modification Development and Physicochemical Characterization of Fast-Dissolving PVA/Poly(ε-caprolactone) Modified with Succinic Acid Films for Oral Drug Delivery Exploration of Multicomponent Triazole-Oxadiazole Clubbed Imidazole Hybrids: Design, Synthesis, In Silico Docking, and DFT Analysis as Potent Pharmacological Agents Amination Reaction on Nickel(II) 3-Nitroazacorroles Synthesis and Study of Antibacterial Activity of Some New Imides Derivatives Containing 1,3,4-Thiadiazole
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1