Enhancing Mechanical Properties of Additively Manufactured H13: A Two-Step Approach Integrating Processing Parameters Optimization and a Tailored Heat Treatment

IF 4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Metals and Materials International Pub Date : 2024-11-13 DOI:10.1007/s12540-024-01808-4
Narges Omidi, Asim Iltaf, Manel Houria, Mohammad Jahazi, Noureddine Barka, Claude Belzile
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Abstract

Rapid solidification during Additive Manufacturing (AM) of H13 steel leads to mesoscopic segregation of alloying elements, which are prone to oxidation during post-AM heat treatment. The presence of oxide particles significantly reduces the tensile strength of powder bed fusion-ed (PBF-ed) H13 steel. The size and distribution of the oxides depend on the selection of both PBF and heat treatment parameters. The purpose of this paper is to maximize the tensile strength of PBF-ed H13, making it comparable to conventional forged and heat treated H13.The research was conducted in two steps. First, PBF processing parameters of laser power, laser speed, hatching space, printing strategy, and preheating temperature were optimized to minimize manufacturing defects and maximize mechanical strength. In the second step, tailored heat treatments were investigated, including annealing at 500 °C for 2 h, quenching at 1020 °C for 1 h, and double tempering at 550 °C for 2 h. Experimental results show that annealing at 500 °C effectively reduces residual stress but does not achieve sufficient elongation. The combination of quenching and tempering significantly enhances elongation to 15% while maintaining a tensile strength of approximately 1517 MPa. This optimized heat treatment strategy also minimized the size and distribution of oxide particles, keeping them under 6 μm in diameter, thereby reducing their detrimental impact on mechanical properties.

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提高增材制造H13的力学性能:工艺参数优化与定制热处理相结合的两步法
H13钢在增材制造过程中的快速凝固导致合金元素的介观偏析,在增材制造后的热处理过程中容易发生氧化。氧化颗粒的存在显著降低了粉末床熔合(PBF-ed) H13钢的拉伸强度。氧化物的大小和分布取决于PBF和热处理参数的选择。本文的目的是最大限度地提高PBF-ed H13的抗拉强度,使其与传统锻造和热处理的H13相媲美。这项研究分两步进行。首先,对激光功率、激光速度、孵化空间、打印策略、预热温度等PBF加工参数进行优化,使制造缺陷最小化,机械强度最大化;在第二步中,研究了定制热处理,包括500℃退火2 h, 1020℃淬火1 h, 550℃双回火2 h。实验结果表明,500℃退火有效降低了残余应力,但没有达到足够的伸长率。淬火和回火相结合可显著提高延伸率至15%,同时保持约1517 MPa的抗拉强度。这种优化的热处理策略还使氧化物颗粒的尺寸和分布最小化,使其直径保持在6 μm以下,从而减少了它们对机械性能的不利影响。图形抽象
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来源期刊
Metals and Materials International
Metals and Materials International 工程技术-材料科学:综合
CiteScore
7.10
自引率
8.60%
发文量
197
审稿时长
3.7 months
期刊介绍: Metals and Materials International publishes original papers and occasional critical reviews on all aspects of research and technology in materials engineering: physical metallurgy, materials science, and processing of metals and other materials. Emphasis is placed on those aspects of the science of materials that are concerned with the relationships among the processing, structure and properties (mechanical, chemical, electrical, electrochemical, magnetic and optical) of materials. Aspects of processing include the melting, casting, and fabrication with the thermodynamics, kinetics and modeling.
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