[dl-Camphor Reference Standard (Control 951) of the National Institute of Health Sciences].

A Kitajima, K Maekawa, K Yoshi, H Komatsu, T Tanimoto, S Okada
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引用次数: 0

Abstract

The raw material of dl-camphor was examined for the preparation of the "dl-Camphor Reference Standard". Analytical data obtained are as follows: ultraviolet spectrum, lambda max = 290 nm; infrared spectrum, the same as that of the present JP Camphor Reference Standard; melting point, 179.6 degrees C; purity test by gas-chromatography (GC), three kinds of impurities were detected; assay by GC, 99.0%. Based on the above results, the candidate raw material was authorized as the JP Reference Standard (Control 951).

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[dl-国家卫生科学研究所樟脑参考标准(Control 951)]。
为编制“dl-樟脑标准品”,对dl-樟脑原料进行了考察。得到的分析数据如下:紫外光谱,λ max = 290 nm;红外光谱,与现行JP樟脑参考标准相同;熔点:179.6℃;气相色谱(GC)纯度检测,检测出3种杂质;气相色谱法,99.0%。根据上述结果,该候选原料被批准为JP参考标准(Control 951)。
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