Analytical methods for the determination of fluoroquinolones in solid environmental matrices

IF 12 1区 化学 Q1 CHEMISTRY, ANALYTICAL Trends in Analytical Chemistry Pub Date : 2011-09-01 DOI:10.1016/j.trac.2011.04.011
Andrea Speltini, Michela Sturini, Federica Maraschi, Antonella Profumo, Angelo Albini
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引用次数: 76

Abstract

We present a critical review of the analytical procedures proposed in the past decade for the determination of fluoroquinolones (FQs) by chromatographic methods in solid environmental matrices. We emphasize the overall analytical procedure, from sampling to final detection. We devote special attention to sample preparation, highlighting the problems involved in the analysis of real complex matrices, mainly soil, sediment, manure and sludge. We compare the different extraction techniques in terms of efficiency, time taken and environmental impact, pointing out advantages and drawbacks. We provide an overview on the role of photochemistry in the degradation of FQs in soils and sediments, and we underline the central position of analytical chemistry in environmental monitoring because FQs are emerging pollutants.

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固体环境基质中氟喹诺酮类药物的测定方法
本文对近十年来固体环境基质中氟喹诺酮类药物的色谱分析方法进行了综述。我们强调从取样到最终检测的整体分析过程。我们特别关注样品制备,重点介绍了实际复杂基质分析中涉及的问题,主要是土壤,沉积物,粪便和污泥。我们比较了不同的提取技术在效率、时间和环境影响方面,指出了优点和缺点。我们概述了光化学在土壤和沉积物中FQs降解中的作用,并强调了分析化学在环境监测中的中心地位,因为FQs是新兴的污染物。
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来源期刊
Trends in Analytical Chemistry
Trends in Analytical Chemistry 化学-分析化学
CiteScore
20.00
自引率
4.60%
发文量
257
审稿时长
3.4 months
期刊介绍: TrAC publishes succinct and critical overviews of recent advancements in analytical chemistry, designed to assist analytical chemists and other users of analytical techniques. These reviews offer excellent, up-to-date, and timely coverage of various topics within analytical chemistry. Encompassing areas such as analytical instrumentation, biomedical analysis, biomolecular analysis, biosensors, chemical analysis, chemometrics, clinical chemistry, drug discovery, environmental analysis and monitoring, food analysis, forensic science, laboratory automation, materials science, metabolomics, pesticide-residue analysis, pharmaceutical analysis, proteomics, surface science, and water analysis and monitoring, these critical reviews provide comprehensive insights for practitioners in the field.
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