Study of X-ray topography using the super-Borrmann effect.

IF 2.4 3区 物理与天体物理 Q2 INSTRUMENTS & INSTRUMENTATION Journal of Synchrotron Radiation Pub Date : 2022-09-01 Epub Date: 2022-08-17 DOI:10.1107/S1600577522007779
J Matsui, K Takatsu, Y Tsusaka
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Abstract

X-ray topography exerting the super-Borrmann effect has been performed using synchrotron radiation to display dislocation images with a high-speed and high-resolution CMOS camera. Forward-transmitted X-rays are positively employed instead of reflected X-rays to reveal dislocations in relatively thick crystals by simultaneously exciting a pair of adjacent {111} planes owing to the super-Borrmann effect. Before the experiment, minimum values of the attenuation coefficients AminP for σ and π polarizations of the incident X-rays in the three-beam case are calculated. Results demonstrate that AminP for both polarizations are almost 20 times larger than those in the two-beam (usual Borrmann effect) case. The transmitted X-rays can be used to confirm the efficacy of taking topographs under the super-Borrmann conditions, as well as under multiple-diffraction conditions. Furthermore, super-Borrmann topographs can be considered for relatively thick crystals, where a conventional Lang X-ray topography technique is difficult to apply.

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利用超玻尔曼效应研究x射线形貌。
利用同步辐射,利用高速高分辨率CMOS相机,利用超博尔曼效应进行了位错图像的x射线形貌研究。由于超博尔曼效应,正透射x射线代替反射x射线,通过同时激发一对相邻的{111}平面来揭示相对厚的晶体中的位错。实验前,计算了三束入射x射线的σ偏振和π偏振的衰减系数AminP的最小值。结果表明,两种偏振下的氨磷比双光束(通常的博尔曼效应)下的氨磷大近20倍。透射x射线可以用来证实在超borrmann条件下以及在多重衍射条件下拍摄地形的有效性。此外,对于相对较厚的晶体,可以考虑采用超borrmann形貌,而传统的Lang x射线形貌技术难以应用。
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来源期刊
CiteScore
5.10
自引率
12.00%
发文量
289
审稿时长
4-8 weeks
期刊介绍: Synchrotron radiation research is rapidly expanding with many new sources of radiation being created globally. Synchrotron radiation plays a leading role in pure science and in emerging technologies. The Journal of Synchrotron Radiation provides comprehensive coverage of the entire field of synchrotron radiation and free-electron laser research including instrumentation, theory, computing and scientific applications in areas such as biology, nanoscience and materials science. Rapid publication ensures an up-to-date information resource for scientists and engineers in the field.
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