[Analysis of Volatile Components and Special Aroma in Fresh Roots of Codonopsis Radix].

中药材 Pub Date : 2016-09-01

{"title":"[Analysis of Volatile Components and Special Aroma in Fresh Roots of Codonopsis Radix].","authors":"","doi":"","DOIUrl":null,"url":null,"abstract":"Objective: To analyze volatile components and special aroma in fresh roots of Codonopsis Radix.Methods: Volatile components in fresh Codonopsis Radix origined from three plant sources were analyzed by HS-GC-MS, and n-hexanal, 2-hexenal and n-hexanol were quantified by HS-GC.Results: 64 constituents have been identified in Codonopsis Radix,which containing ten alcohol,20 aldehyde,14 terpene, three ketone, four ester, four furan, three acid, one olefin, one alkane, two sulfide and two other compounds. The total percentage of n-hexanal,2-hexenal and n-hexanol was large, which were the main volatile compounds in Codonopsis Radix. The content of n-hexanal in Lu Dangshen, Baitiao Dangshen, Wen Dangshen, Feng Dangshen and Banqiao Dangshen were 54. 89%,59. 01%,55. 07%,42. 42% and 56. 74%,which were the major volatile component contributing to special aroma in Codonopsis Radix. 61 compounds have been identified in Lu Dangshen including 8 specific compounds. An external calibration method was established for simultaneous determination of n-hexanal,2-hexenal and hexanol in Codonopsis Radix. The results showed that all calibration curve three volatile components exhibited good linearity at a range of concentrations( R2≥0. 9995). The recoveries of n-hexanal, 2-hexenal and hexanol were 100. 1%,94. 8% and 112. 6%,and the RSD were 4. 4%,8. 7% and 8. 1%,respectively. The analysis suggested that the content of n-hexanal in Lu Dangshen was 200. 41 μg / g and significantly higher than that in Banqiao Dangshen, Wen Dangshen and Feng Dangshen while similar to Baitiao Dangshen. The content of hexanol in three-year-old Lu Dangshen was significantly higher than that in twoyear-old Lu Dangshen.Conclusion: The present research indicates that special aroma is an important feature of authentic Dangshen.","PeriodicalId":15312,"journal":{"name":"中药材","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2016-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"中药材","FirstCategoryId":"3","ListUrlMain":"","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}

引用次数: 0

Abstract

Objective: To analyze volatile components and special aroma in fresh roots of Codonopsis Radix.

Methods: Volatile components in fresh Codonopsis Radix origined from three plant sources were analyzed by HS-GC-MS, and n-hexanal, 2-hexenal and n-hexanol were quantified by HS-GC.

Results: 64 constituents have been identified in Codonopsis Radix,which containing ten alcohol,20 aldehyde,14 terpene, three ketone, four ester, four furan, three acid, one olefin, one alkane, two sulfide and two other compounds. The total percentage of n-hexanal,2-hexenal and n-hexanol was large, which were the main volatile compounds in Codonopsis Radix. The content of n-hexanal in Lu Dangshen, Baitiao Dangshen, Wen Dangshen, Feng Dangshen and Banqiao Dangshen were 54. 89%,59. 01%,55. 07%,42. 42% and 56. 74%,which were the major volatile component contributing to special aroma in Codonopsis Radix. 61 compounds have been identified in Lu Dangshen including 8 specific compounds. An external calibration method was established for simultaneous determination of n-hexanal,2-hexenal and hexanol in Codonopsis Radix. The results showed that all calibration curve three volatile components exhibited good linearity at a range of concentrations( R2≥0. 9995). The recoveries of n-hexanal, 2-hexenal and hexanol were 100. 1%,94. 8% and 112. 6%,and the RSD were 4. 4%,8. 7% and 8. 1%,respectively. The analysis suggested that the content of n-hexanal in Lu Dangshen was 200. 41 μg / g and significantly higher than that in Banqiao Dangshen, Wen Dangshen and Feng Dangshen while similar to Baitiao Dangshen. The content of hexanol in three-year-old Lu Dangshen was significantly higher than that in twoyear-old Lu Dangshen.

Conclusion: The present research indicates that special aroma is an important feature of authentic Dangshen.

微信好友朋友圈 QQ好友复制链接

本刊更多论文

鲜党参根挥发性成分及特殊香气分析

目的:分析鲜党参根的挥发性成分及特有香气。方法:采用HS-GC- ms对三种植物来源的新鲜党参挥发物成分进行分析，并采用HS-GC对正己醛、2-己烯醛和正己醇进行定量分析。结果:共鉴定出党参成分64种，其中醇10种，醛20种，萜14种，酮3种，酯4种，呋喃4种，酸3种，烯烃1种，烷烃1种，硫化物2种，其他化合物2种。正己醛、2-己烯醛和正己醇总含量较高，是党参中主要挥发性成分。鹿党参、白条党参、文党参、凤党参、板桥党参的正己醛含量为54。89%, 59岁。01%, 55。07%, 42。42%和56%。在芦党参中共鉴定出61种化合物，其中特异性化合物8种。建立了同时测定党参中正己醛、2-己醛和己醇含量的外标方法。结果表明，3种挥发性成分在浓度范围内均呈良好的线性关系(R2≥0)。9995)。正己醛、2-己醛和己醇的加样回收率为100。1%, 94。8%和112。6%， RSD为4。4%, 8。7%和8%。1%,分别。分析表明鹿党参中正己醛的含量为200。41 μg / g，显著高于板桥党参、文党参和凤党参，与白条党参相似。三岁鹿党参中己醇含量显著高于两岁鹿党参。结论:独特的香气是党参正品的重要特征。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

求助全文

约1分钟内获得全文去求助

来源期刊

中药材

自引率

0.00%

发文量

11364

期刊介绍： "Chinese Materia Medica" magazine was founded in 1978. It is a national-level academic journal of Chinese medicine science and technology approved by the State Science and Technology Commission and the Press and Publication Administration for public distribution at home and abroad. It is sponsored by the Chinese Materia Medica Information Center of the State Food and Drug Administration and is publicly distributed at home and abroad. It mainly reports on new technologies, new methods and new achievements in the production, scientific research and business management of Chinese medicine, and serves to promote the production and scientific and technological development of Chinese medicine, improve the output and quality of Chinese medicine, improve business management, and prosper the Chinese medicine industry.