Effect of thermal cycling on temperature changes and bond strength in different test specimens.

Biomaterial investigations in dentistry Pub Date : 2020-01-29 eCollection Date: 2020-01-01 DOI:10.1080/26415275.2019.1709470
Sigfus Thor Eliasson, Jon Einar Dahl
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引用次数: 22

Abstract

Objectives: To investigate temperature changes in various test specimens during thermal cycling and to evaluate difference in micro-tensile repair bond strength in specimens cut from the inner or the outer area of composite blocks after thermal cycling. Materials and methods: Four rectangular composite blocks of various sizes were fabricated, and thermocouples placed in the centre of the specimens or halfway from the surface to the centre. Composite cylinders were made on ground flat extracted molars, as intended for micro-tensile and shear bond testing, with a thermocouple placed at the centre of the cylinder radius between composite and dentin. The specimens were thermal cycled between 5 °C and 55 °C with 20-60 s dwell times. The highest and lowest temperatures in the test specimens were recorded. Composite blocks were fabricated and stored in water for a week and then repaired with the same composite. After thermal cycling (5000×, 5 °C and 55 °C with a 20 s dwell time), test specimens were cut for micro-tensile testing. Results: None of the specimens tested reached the cold and warm water bath temperatures after a 20 s dwell time. In the smallest composite block, the centre core temperature reached 5 °C and 55 °C after 40 s dwell time, but lacked 1 °C after 60 s in the largest block. None of the specimens involving teeth reached water temperatures. The micro-tensile repair strength was significantly different between the outer and the central cut rods (p < .05). Conclusions: The most commonly used dwell times for thermal cycling are insufficient to create a homogeneous temperature change.

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热循环对不同试件温度变化及粘结强度的影响。
目的:研究热循环过程中不同试样的温度变化,评价热循环后复合材料砌块内切和外切试样微拉伸修复粘结强度的差异。材料和方法:制作4个不同尺寸的矩形复合块,热电偶放置在样品的中心或从表面到中心的中间位置。复合圆柱体是在地面平坦的拔牙上制作的,用于微拉伸和剪切粘结测试,热电偶放置在圆柱体半径的中心,介于复合材料和牙本质之间。样品在5℃~ 55℃之间热循环,停留时间20 ~ 60 s。记录了试样的最高和最低温度。将复合材料砌块制作完成,在水中保存一周,然后用相同的复合材料进行修复。热循环(5000x, 5°C和55°C,停留时间20 s)后,切割试样进行微拉伸测试。结果:经20 s静置后,所有试样均未达到冷热水浴温度。在最小的复合块中,停留40 s后中心核心温度达到5°C和55°C,而在最大块中停留60 s后中心核心温度缺乏1°C。所有涉及牙齿的标本都没有达到水温。结论:最常用的热循环停留时间不足以产生均匀的温度变化。
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