Evaluating the Bonding Performance of a Novel Dual-curing Composite Cement to Zirconia.

IF 4.6 Q2 MATERIALS SCIENCE, BIOMATERIALS ACS Applied Bio Materials Pub Date : 2021-12-03 DOI:10.3290/j.jad.b2288181
Yue Yan, Huaiqin Zhang, Jiaxue Yang, Chen Chen
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引用次数: 3

Abstract

Purpose: To investigate the bond strength and durability of a novel dual-curing composite cement to zirconia under different curing conditions.

Materials and methods: Zirconia plates of different thickness (0.5, 1, and 2 mm) were bonded with either a novel dual-curing composite cement (Panavia V5, PV5, Kuraray Noritake) or a traditional one (RelyX Ultimate, RUL, 3M Oral Care; Multilink Automix, MLA, Ivoclar Vivadent), in light-, self-, or dual-curing mode. Bonded specimens were subjected to shear bond strength (SBS) tests after 24 h of water storage or after artificially aging by 20,000 thermal cycles plus 150 days of water storage. The degree of conversion (DC) of the composite cements under different curing conditions was measured by Fourier transform infrared (FTIR) spectroscopy. The irradiance and translucency of the zirconia plates of different thickness were also investigated.

Results: The irradiance and translucency of zirconia decreased significantly with increasing thickness (p = 0.00). Both before and after aging, SBS of PV5 in self-curing mode was significantly higher than that of RUL (p = 0.07 before aging and 0.02 after aging) and MLA (p = 0.00 both before and after aging). However, for the three composite cements, light- and dual curing yielding the same SBSs for a constant Y-TZP thickness (p > 0.05). The FTIR analysis showed that, for all three dual-curing composite cements examined in this study, the mean DC values obtained in dual-curing mode were lower than those achieved in light-curing mode (p = 0.00 for PV5, RUL, and MLA). For RUL and MLA, lower mean DC values were obtained in self-curing than dual-curing mode (p = 0.00 for both RUL and MLA), while the DC values of PV5 showed no significant difference between self-curing and dual-curing mode (p = 0.33).

Conclusion: When the photoactivation time is 60 s and the thickness of the zirconia restoration is less than 2 mm, it is safe to use the two traditional dual-curing composite cements RUL and MLA and PV5 for bonding zirconia. However, when the light exposure time is insufficient, PV5 provides improved bond strength and durability to zirconia.

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新型双固化Composite水泥与氧化锆的粘结性能评价。
目的:研究新型双固化composite水泥与氧化锆在不同固化条件下的粘结强度和耐久性。材料和方法:将不同厚度的氧化锆板(0.5,1和2mm)与新型双固化复合水泥(Panavia V5, pv5_, Kuraray Noritake)或传统复合水泥(RelyX Ultimate, rul_, 3M Oral Care;多链接自动,mla_, ivclar Vivadent),在光,自,或双固化模式。试件在蓄水24 h或人工老化2万次热循环加蓄水150 d后进行剪切粘结强度(SBS)试验。采用傅里叶红外光谱法测定了复合水泥在不同固化条件下的转化率(DC)。研究了不同厚度氧化锆板的辐照度和透光率。结果:氧化锆的辐照度和透明度随厚度的增加而显著降低(p = 0.00)。在老化前后,自固化模式下SBS of PV5 was均显著高于RUL(老化前p = 0.07,老化后p = 0.02)和MLA(老化前后p = 0.00)的that。然而,对于三种复合水泥,在Y-TZP厚度恒定的情况下,光固化和双固化产生相同的SBSs (p > 0.05)。FTIR分析显示,对于本研究中检测的所有三种双固化复合水泥,双固化模式下获得的平均DC值低于光固化模式下获得的DC值(PV5、RUL和MLA的p = 0.00)。对于RUL和MLA,自固化的平均DC值低于双固化模式(RUL和MLA均p = 0.00),而PV5的DC值在自固化和双固化模式之间无显著差异(p = 0.33)。结论:当光活化时间为60 s,氧化锆修复体厚度小于2 mm时,使用两种传统的双固化复合水泥RUL和MLA + PV5粘结氧化锆是安全的。然而,当光照时间不足时,PV5可以提高氧化锆的结合强度和耐久性。
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来源期刊
ACS Applied Bio Materials
ACS Applied Bio Materials Chemistry-Chemistry (all)
CiteScore
9.40
自引率
2.10%
发文量
464
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