Comparison between heat treatment and SPS treatment on CoCrFeMnNi/WC coatings

IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, COATINGS & FILMS Surface Engineering Pub Date : 2022-09-02 DOI:10.1080/02670844.2022.2154033
Yicheng Zhou, Bing-Jiang Yang, Guo Zhang
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引用次数: 1

Abstract

ABSTRACT In this study, spark plasma sintering (SPS) was used for the thermoelectric composite treatment of CrMnFeCoNi/WC plasma transfer arc welding (PTA) coating to explore the difference compared with common heat treatment (HT). X-ray diffraction (XRD) was used to detect the phase composition, and a combination of scanning electron microscopy (SEM) and transmission electron microscopy (TEM) was used to characterize the microstructure. The performance of nano-indentation was tested. The results show that the coating after PTA has a large dislocation density due to internal stress, while HT and SPS treatment significantly reduce the internal stress and dislocation density of the coating. Nano-indentation test shows that the hardness of the coating after PTA is 4.24 GPa, and after HT, the hardness decreases to 4.05 GPa. However, the coating after SPS treatment has significant precipitation-strengthening effect due to the wide existence of the precipitated phase, and the hardness rises to 4.78 GPa.
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CoCrFeMnNi/WC涂层热处理与SPS处理的比较
摘要本研究采用火花等离子体烧结(SPS)对CrMnFeCoNi/WC等离子转移焊(PTA)涂层进行热电复合处理,以探讨其与普通热处理(HT)的差异。使用X射线衍射(XRD)检测相组成,并使用扫描电子显微镜(SEM)和透射电子显微镜(TEM)的组合来表征微观结构。测试了纳米压痕的性能。结果表明,PTA处理后的涂层由于内应力而具有较大的位错密度,而HT和SPS处理显著降低了涂层的内应力和位错密度。纳米压痕试验表明,PTA后涂层的硬度为4.24 GPa,HT后硬度降至4.05 GPa。然而,SPS处理后的涂层由于沉淀相的广泛存在,具有显著的沉淀强化效果,硬度提高到4.78 GPa。
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来源期刊
Surface Engineering
Surface Engineering 工程技术-材料科学:膜
CiteScore
5.60
自引率
14.30%
发文量
51
审稿时长
2.3 months
期刊介绍: Surface Engineering provides a forum for the publication of refereed material on both the theory and practice of this important enabling technology, embracing science, technology and engineering. Coverage includes design, surface modification technologies and process control, and the characterisation and properties of the final system or component, including quality control and non-destructive examination.
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