Supersolidus Sintering of Cr Prealloyed Steels by Inductive Heating

Q4 Materials Science Powder Metallurgy Progress Pub Date : 2019-12-01 DOI:10.1515/pmp-2019-0006
C. Gierl-Mayer, M. Huemer, H. Danninger, M. Dlapka, G. Stetina, R. Ratzi
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Abstract

Abstract For powder metallurgy products, high density is an essential requirements to obtain maximum mechanical properties. Here, supersolidus liquid phase sintering (SSPLS) is an effective means to attain high sintered density, as known from PM high speed steels. In the present work it is shown that this technique can also be applied to Cr prealloyed low alloy steel grades. Supersolidus sintering through indirect heating requires precise control of temperature and also the atmosphere, to avoid uncontrolled changes of the carbon level. Higher C contents are beneficial here since they enable lower temperatures and result in wider temperature windows for sintering. The temperatures necessary for SSLPS at moderate C levels are fairly high for standard sintering furnaces, therefore induction sintering was studied in this work. It showed that, as was to be expected, also here precise temperature control is required, but for any carbon level tested a sintering temperature could be identified that yielded high sintered density and good shape retention. The high density attained, in combination with the very high temperatures, results in pronounced grain growth, this process no more being inhibited by the presence of pores, which is undesirable but can however be remedied by suitable heat treatment.
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感应加热Cr预合金钢的超固相烧结
摘要对于粉末冶金产品来说,高密度是获得最大机械性能的基本要求。在这里,超固相液相烧结(SSPLS)是获得高烧结密度的有效手段,正如从PM高速钢中已知的那样。本工作表明,该技术也可应用于Cr预合金低合金钢牌号。通过间接加热的超固体烧结需要精确控制温度和大气,以避免碳含量的不可控变化。较高的C含量在这里是有益的,因为它们能够实现较低的温度并导致更宽的烧结温度窗口。对于标准烧结炉来说,在中等C水平下进行SSLPS所需的温度相当高,因此本文对感应烧结进行了研究。结果表明,正如预期的那样,这里也需要精确的温度控制,但对于任何测试的碳水平,都可以确定烧结温度,该温度产生高的烧结密度和良好的形状保持性。所获得的高密度与非常高的温度相结合,导致显著的晶粒生长,这一过程不再受到孔隙存在的抑制,这是不希望的,但可以通过适当的热处理来补救。
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Powder Metallurgy Progress
Powder Metallurgy Progress Materials Science-Metals and Alloys
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