首页 > 最新文献

Powder Metallurgy Progress最新文献

英文 中文
Announcements: Professor RNDr. Ján Dusza, DrSc – 70 years jubeeleum 公告:RNDr.教授。Ján Dusza,博士–70岁
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0001
{"title":"Announcements: Professor RNDr. Ján Dusza, DrSc – 70 years jubeeleum","authors":"","doi":"10.2478/pmp-2022-0001","DOIUrl":"https://doi.org/10.2478/pmp-2022-0001","url":null,"abstract":"","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49067954","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Micromechanical Properties of Reactive HiTUS TiNbVTaZrHf–N Coatings on Different Substrates 不同基材上反应性HiTUS TiNbVTaZrHf-N涂层的微观力学性能
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0005
František Lofaj, Tamás Csanádi, Lenka Kvetková, Petra Hviščová, Margita Kabátová, Alexandra Kovalčíková, Marek Vojtko, Vladimir Girman
Abstract High entropy ceramic coatings, including multicomponent transition metal nitrides called also high entropy nitrides (HEN), are usually deposited using reactive arc and/or DC magnetron (co)sputtering. High Target Utilization Sputtering (HiTUS) was not applied in HEN systems up to now. Subsequently, the mechanical properties of HEN coatings prepared by HiTUS are also not known. The transition metals from the 4 th and 5 th group of the periodic table (Ti, Zr, Hf, Nb, V, and Ta) are strong nitride formers which would be the most suitable for HEN coating systems and therefore, investigation of their properties would be of significant interest. However, the nanoindentation measurements on thin coatings always produce „composite“ values involving the contribution from the substrate. The separation of the coating properties from composite values requires upgraded analytical approaches different from standard Oliver & Pharr analysis. Thus, the aim work is to investigate the structure, hardness, and elastic modulus of TiZrHfNbVTa–xN coatings with different nitrogen stoichiometry deposited by reactive HiTUS using both CSM for bulk and CSM for thin films methods and to compare the results obtained on 4 different substrates (Si wafer, sapphire, 100Cr6 steel, and Ti6Al4V alloy). The subsequent results showed systematic differences in the calculated mechanical properties depending on the substrate properties both in CSM and CSMTF modes. Stiffer substrates always resulted in the overestimations of the calculated hardness and indentation modulus compared to softer substrates with lower Young’s modulus and the differences were in the range of around 10 %. Obviously, better theoretical models for the calculations of true coating properties are required.
高熵陶瓷涂层,包括多组分过渡金属氮化物,也称为高熵氮化物(HEN),通常采用反应电弧和/或直流磁控(co)溅射沉积。高目标利用率溅射(HiTUS)技术目前尚未应用于HEN系统。随后,利用HiTUS制备的HEN涂层的力学性能也不得而知。元素周期表第4和第5族的过渡金属(Ti, Zr, Hf, Nb, V和Ta)是强氮化物形成物,最适合用于HEN涂层系统,因此,研究它们的性能将是一个重要的兴趣。然而,对薄涂层的纳米压痕测量总是产生“复合”值,包括基底的贡献。从复合值中分离涂层性能需要升级的分析方法,不同于标准的Oliver &法尔分析。因此,本研究的目的是研究不同氮化学计量的TiZrHfNbVTa-xN涂层的结构、硬度和弹性模量,并比较在4种不同衬底(硅片、蓝宝石、100Cr6钢和Ti6Al4V合金)上沉积的结果。随后的结果表明,在CSM和CSMTF模式下,计算得到的力学性能存在系统差异。与杨氏模量较低的较软的基材相比,较硬的基材总是导致计算硬度和压痕模量的高估,差异在10%左右。显然,需要更好的理论模型来计算涂层的真实性能。
{"title":"Micromechanical Properties of Reactive HiTUS TiNbVTaZrHf–N Coatings on Different Substrates","authors":"František Lofaj, Tamás Csanádi, Lenka Kvetková, Petra Hviščová, Margita Kabátová, Alexandra Kovalčíková, Marek Vojtko, Vladimir Girman","doi":"10.2478/pmp-2022-0005","DOIUrl":"https://doi.org/10.2478/pmp-2022-0005","url":null,"abstract":"Abstract High entropy ceramic coatings, including multicomponent transition metal nitrides called also high entropy nitrides (HEN), are usually deposited using reactive arc and/or DC magnetron (co)sputtering. High Target Utilization Sputtering (HiTUS) was not applied in HEN systems up to now. Subsequently, the mechanical properties of HEN coatings prepared by HiTUS are also not known. The transition metals from the 4 th and 5 th group of the periodic table (Ti, Zr, Hf, Nb, V, and Ta) are strong nitride formers which would be the most suitable for HEN coating systems and therefore, investigation of their properties would be of significant interest. However, the nanoindentation measurements on thin coatings always produce „composite“ values involving the contribution from the substrate. The separation of the coating properties from composite values requires upgraded analytical approaches different from standard Oliver & Pharr analysis. Thus, the aim work is to investigate the structure, hardness, and elastic modulus of TiZrHfNbVTa–xN coatings with different nitrogen stoichiometry deposited by reactive HiTUS using both CSM for bulk and CSM for thin films methods and to compare the results obtained on 4 different substrates (Si wafer, sapphire, 100Cr6 steel, and Ti6Al4V alloy). The subsequent results showed systematic differences in the calculated mechanical properties depending on the substrate properties both in CSM and CSMTF modes. Stiffer substrates always resulted in the overestimations of the calculated hardness and indentation modulus compared to softer substrates with lower Young’s modulus and the differences were in the range of around 10 %. Obviously, better theoretical models for the calculations of true coating properties are required.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135195314","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Fracture Toughness of Cement Paste Assessed with Micro-Scratch and Acoustic Emission 用微划痕和声发射评价水泥浆体的断裂韧性
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0002
J. Němeček, R. Čtvrtlík, L. Václavek
Abstract Micro-scratch test was used to evaluate the fracture toughness of the main hydration products of ordinary Portland cement paste at the micro-scale. The evaluation was done with the aid of scanning electron microscopy and acoustic emission (AE) signals. Portlandite was found to be the only phase where AE detected elastic waves due to cracking during microindentation and micro-scratch test. Such behavior simplifies phase separation during the evaluation process of the micro-scratch test. The micro-scale fracture toughness results obtained from the tests were found in close agreement with other available experiments and models in the literature.
摘要采用微划伤试验对普通硅酸盐水泥浆体主要水化产物在微尺度下的断裂韧性进行了评价。利用扫描电镜和声发射(AE)信号对其进行了评价。在微压痕和微划痕试验中,波特兰岩是唯一能探测到裂纹引起的弹性波的阶段。这种行为简化了微划痕试验评价过程中的相分离。从试验中得到的微尺度断裂韧性结果与文献中其他可用的实验和模型非常吻合。
{"title":"Fracture Toughness of Cement Paste Assessed with Micro-Scratch and Acoustic Emission","authors":"J. Němeček, R. Čtvrtlík, L. Václavek","doi":"10.2478/pmp-2022-0002","DOIUrl":"https://doi.org/10.2478/pmp-2022-0002","url":null,"abstract":"Abstract Micro-scratch test was used to evaluate the fracture toughness of the main hydration products of ordinary Portland cement paste at the micro-scale. The evaluation was done with the aid of scanning electron microscopy and acoustic emission (AE) signals. Portlandite was found to be the only phase where AE detected elastic waves due to cracking during microindentation and micro-scratch test. Such behavior simplifies phase separation during the evaluation process of the micro-scratch test. The micro-scale fracture toughness results obtained from the tests were found in close agreement with other available experiments and models in the literature.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42424319","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Evaluation of Residual Stress and Tensile Properties of Railway Axle Using Instrumented Indentation Method 用仪器压痕法评价铁路车轴的残余应力和拉伸性能
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0003
D. Bartonek, M. Négyesi, B. Strnadel
Abstract This paper deals with the characterization of residual stresses of the railway axle made of EA4T steel using the instrumented indentation technique (IIT). Additionally, tensile properties were also evaluated by using IIT. Moreover, the hole drilling method was carried out to measure the residual stress. Multiple comparison tests between conventional methods and IIT were carried out. The obtained results were also discussed against the literature data. Results of the residual stress assessed by IIT and the hole drilling follow the same trend and are in acceptable agreement. The tensile data obtained by IIT were as follows: YS ≥ 420 MPa and UTS ∈ ❬650-800❭MPa which is in satisfactory agreement with the results of standardized tensile tests.
本文采用仪器压痕技术(IIT)对EA4T钢制铁路车轴的残余应力进行了表征。此外,还使用IIT对拉伸性能进行了评估。此外,还采用钻孔法测量了残余应力。对传统方法和IIT进行了多次比较试验。并结合文献资料对所得结果进行了讨论。IIT和钻孔评估的残余应力结果遵循相同的趋势,且一致性可接受。IIT得到的拉伸数据如下:YS≥420MPa❬650-800❭MPa,这与标准化拉伸试验的结果一致。
{"title":"Evaluation of Residual Stress and Tensile Properties of Railway Axle Using Instrumented Indentation Method","authors":"D. Bartonek, M. Négyesi, B. Strnadel","doi":"10.2478/pmp-2022-0003","DOIUrl":"https://doi.org/10.2478/pmp-2022-0003","url":null,"abstract":"Abstract This paper deals with the characterization of residual stresses of the railway axle made of EA4T steel using the instrumented indentation technique (IIT). Additionally, tensile properties were also evaluated by using IIT. Moreover, the hole drilling method was carried out to measure the residual stress. Multiple comparison tests between conventional methods and IIT were carried out. The obtained results were also discussed against the literature data. Results of the residual stress assessed by IIT and the hole drilling follow the same trend and are in acceptable agreement. The tensile data obtained by IIT were as follows: YS ≥ 420 MPa and UTS ∈ ❬650-800❭MPa which is in satisfactory agreement with the results of standardized tensile tests.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46648632","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
The Influence of Tilt on Berkovich Indentation of a Steel Sample Using FEM Analysis and Nanoindentation 利用有限元分析和纳米压痕研究倾斜对钢试样Berkovich压痕的影响
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0007
Jaroslav Kovář, Vladimír Fuis, Radim Čtvrtlík, Jan Tomáštík
Abstract The main shape deviations of a Berkovich indenter are the indenter bluntness and indenter tilt. The influence of the Berkovich indenter tilt on the results of the FEM modelling of steel nanoindentation is evaluated in this paper. The indenter tilt has an impact on the indentation curves and contact area. The X5CrNiCuNb 16-4 steel nanoindentation was modelled by FEM and the indentation curves were obtained. The Berkovich indenter was blunted and the tilt of the indenter was changed to determine its influence on the indentation curves. The results showed that growing tilt shifts the indentation curves to higher values of indentation forces and makes unloading curves steeper which is in agreement with a larger contact area. The calculated indentation curves were compared with the experimental indentation curves and the impact of the indenter tilt to the indentation curves was determined.
摘要伯氏压头的主要形状偏差是压头钝度和压头倾斜度。本文评价了Berkovich压头倾角对钢纳米压痕有限元模拟结果的影响。压痕倾斜对压痕曲线和接触面积有影响。采用有限元法模拟了X5CrNiCuNb 16-4钢的纳米压痕,得到了压痕曲线。将伯氏压头钝化,并改变压头的倾斜度,以确定其对压痕曲线的影响。结果表明:随着倾斜度的增大,压痕曲线的压痕力值增大,卸载曲线变陡,这与较大的接触面积相一致;将计算得到的压痕曲线与实验得到的压痕曲线进行了比较,确定了压痕倾斜对压痕曲线的影响。
{"title":"The Influence of Tilt on Berkovich Indentation of a Steel Sample Using FEM Analysis and Nanoindentation","authors":"Jaroslav Kovář, Vladimír Fuis, Radim Čtvrtlík, Jan Tomáštík","doi":"10.2478/pmp-2022-0007","DOIUrl":"https://doi.org/10.2478/pmp-2022-0007","url":null,"abstract":"Abstract The main shape deviations of a Berkovich indenter are the indenter bluntness and indenter tilt. The influence of the Berkovich indenter tilt on the results of the FEM modelling of steel nanoindentation is evaluated in this paper. The indenter tilt has an impact on the indentation curves and contact area. The X5CrNiCuNb 16-4 steel nanoindentation was modelled by FEM and the indentation curves were obtained. The Berkovich indenter was blunted and the tilt of the indenter was changed to determine its influence on the indentation curves. The results showed that growing tilt shifts the indentation curves to higher values of indentation forces and makes unloading curves steeper which is in agreement with a larger contact area. The calculated indentation curves were compared with the experimental indentation curves and the impact of the indenter tilt to the indentation curves was determined.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135195315","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Investigation of Hybrid Lap Welds of TI6AL4V and Stainless Steel with Bronze Interlayer TI6AL4V与不锈钢复合搭接焊青铜夹层的研究
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0006
Hana Chmelíčková, Martina Havelková, Aneta Hrubantová, Vlastimil Jílek, Lukáš Václavek, Tomáš Ingr
Abstract Welding of the austenitic stainless steel AISI 304 and Ti6Al4V is complicated by hard and brittle intermetallic compound formation. In this contribution, we study a laser welding method that partially overcomes this problem using interlayer. Bronze foil (CuSn6) of thickness 100 µm and 200 µm was inserted between steel and titanium sheets and lap welds were realized on pulsed Nd:YAG laser. Representative samples were investigated by nanohardness measurement, SEM/EDS, and XRD analysis to detect the localization of the intermetallic phases. The macrostructure of the weld cross sections was displayed by optical and digital microscopy. The nano-hardness test revealed the presence of very hard intermetallic mainly around the interface between the fusion zone and bottom metal sheet. EDS mapping displayed the main elements Fe, Cr, Cu and Ti distribution in the fusion zone, EDS line scanning detected elements‘ signals in the diagonal and horizontal directions. XRD analysis revealed expected intermetallic compounds FeTi and CuTi 2 and solid solution Cu 0.8 Fe 0.2 .
奥氏体不锈钢AISI 304与Ti6Al4V的焊接过程中会形成硬脆的金属间化合物。在本文中,我们研究了一种使用中间层的激光焊接方法,部分地克服了这一问题。采用脉冲Nd:YAG激光将厚度分别为100µm和200µm的铜箔(CuSn6)插入钢和钛板之间,实现了接焊。采用纳米硬度测定、SEM/EDS、XRD分析等方法对代表性样品进行了金属间相定位分析。通过光学显微镜和数码显微镜观察了焊缝截面的宏观组织。纳米硬度测试表明,极硬金属间主要存在于熔合区与底金属板交界面周围。能谱图显示了熔合区内主要元素Fe、Cr、Cu和Ti的分布,能谱线扫描在对角线和水平方向检测到元素的信号。XRD分析表明,金属间化合物为FeTi和CuTi 2,固溶体为Cu 0.8 Fe 0.2。
{"title":"Investigation of Hybrid Lap Welds of TI6AL4V and Stainless Steel with Bronze Interlayer","authors":"Hana Chmelíčková, Martina Havelková, Aneta Hrubantová, Vlastimil Jílek, Lukáš Václavek, Tomáš Ingr","doi":"10.2478/pmp-2022-0006","DOIUrl":"https://doi.org/10.2478/pmp-2022-0006","url":null,"abstract":"Abstract Welding of the austenitic stainless steel AISI 304 and Ti6Al4V is complicated by hard and brittle intermetallic compound formation. In this contribution, we study a laser welding method that partially overcomes this problem using interlayer. Bronze foil (CuSn6) of thickness 100 µm and 200 µm was inserted between steel and titanium sheets and lap welds were realized on pulsed Nd:YAG laser. Representative samples were investigated by nanohardness measurement, SEM/EDS, and XRD analysis to detect the localization of the intermetallic phases. The macrostructure of the weld cross sections was displayed by optical and digital microscopy. The nano-hardness test revealed the presence of very hard intermetallic mainly around the interface between the fusion zone and bottom metal sheet. EDS mapping displayed the main elements Fe, Cr, Cu and Ti distribution in the fusion zone, EDS line scanning detected elements‘ signals in the diagonal and horizontal directions. XRD analysis revealed expected intermetallic compounds FeTi and CuTi 2 and solid solution Cu 0.8 Fe 0.2 .","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135195316","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of Machining on Mechanical Properties of Borosilicate Glasses 加工对硼硅酸盐玻璃力学性能的影响
Q4 Materials Science Pub Date : 2023-06-01 DOI: 10.2478/pmp-2022-0008
Lukáš Václavek, Jan Tomáštík, Radim Čtvrtlík
Abstract Although optical properties are essential for materials for optical purposes, their mechanical properties must also be considered as they directly govern their practical applicability as well as their machining. The machining of optical glasses is mainly carried out by mechanical removal of the material using free or bonded abrasives. The relationship between the local mechanical properties of three types of borosilicate glasses used to produce optical elements (mirrors) and the type of surface machining was investigated. The samples were machined using two approaches, namely 7-axis CNC surface machining and conventional manual machining. Advanced analysis of nano/micro-mechanical properties was performed on glass samples using quasi-static nanoindentation and microindentation and dynamic impact test complemented by the analysis of the acoustic emission signals generated during the mechanical tests. The results show a difference in mechanical properties between industrial and optical borosilicate glasses. The type of machining has a strong influence on studied mechanical properties and surface quality. Glasses manufactured by CNC have more pronounced acoustic emission signal and crack more than glasses manufactured by hand. The different behavior of hand- and CNC-machined surfaces can be linked to different subsurface damage caused by different contact conditions between the workpiece and the instrument/abrasive. As a result, a different density of surface and especially (near)-subsurface flaws are present in the glass. Simax is slightly softer than BG33 glass, which together with the less pronounced AE may indicate a lower amount of subsurface cracks/damage.
虽然光学性能是光学材料的基本要求,但其机械性能也必须考虑,因为它直接决定了材料的实际适用性和加工。光学玻璃的加工主要是通过使用自由或粘合磨料机械去除材料来进行的。研究了三种光学元件(反射镜)用硼硅酸盐玻璃的局部力学性能与表面加工方式的关系。采用7轴数控平面加工和常规手工加工两种加工方式对样品进行加工。利用准静态纳米压痕、微压痕和动态冲击试验对玻璃样品的纳米/微力学性能进行了深入分析,并对力学试验过程中产生的声发射信号进行了分析。结果表明,工业硼硅酸盐玻璃与光学硼硅酸盐玻璃在力学性能上存在差异。加工方式对所研究的机械性能和表面质量有很大影响。数控加工的玻璃声发射信号比手工加工的更明显,裂纹也更大。手工和cnc加工表面的不同行为可能与工件与仪器/磨料之间的不同接触条件造成的不同亚表面损伤有关。结果,不同密度的表面,特别是(近)表面下的缺陷存在于玻璃中。Simax比BG33玻璃稍软,再加上声发射不太明显,可能表明表面下裂纹/损伤的数量较少。
{"title":"Effect of Machining on Mechanical Properties of Borosilicate Glasses","authors":"Lukáš Václavek, Jan Tomáštík, Radim Čtvrtlík","doi":"10.2478/pmp-2022-0008","DOIUrl":"https://doi.org/10.2478/pmp-2022-0008","url":null,"abstract":"Abstract Although optical properties are essential for materials for optical purposes, their mechanical properties must also be considered as they directly govern their practical applicability as well as their machining. The machining of optical glasses is mainly carried out by mechanical removal of the material using free or bonded abrasives. The relationship between the local mechanical properties of three types of borosilicate glasses used to produce optical elements (mirrors) and the type of surface machining was investigated. The samples were machined using two approaches, namely 7-axis CNC surface machining and conventional manual machining. Advanced analysis of nano/micro-mechanical properties was performed on glass samples using quasi-static nanoindentation and microindentation and dynamic impact test complemented by the analysis of the acoustic emission signals generated during the mechanical tests. The results show a difference in mechanical properties between industrial and optical borosilicate glasses. The type of machining has a strong influence on studied mechanical properties and surface quality. Glasses manufactured by CNC have more pronounced acoustic emission signal and crack more than glasses manufactured by hand. The different behavior of hand- and CNC-machined surfaces can be linked to different subsurface damage caused by different contact conditions between the workpiece and the instrument/abrasive. As a result, a different density of surface and especially (near)-subsurface flaws are present in the glass. Simax is slightly softer than BG33 glass, which together with the less pronounced AE may indicate a lower amount of subsurface cracks/damage.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135195313","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of Sintering Time on Mechanical Properties of (Hf-Ta-Zr-Nb-Ti)C 烧结时间对(Hf-Ta-Zr-Nb-Ti)C力学性能的影响
Q4 Materials Science Pub Date : 2021-12-01 DOI: 10.2478/pmp-2021-0006
Lenka Ďaková, M. Hrubovčáková, R. Sedlák, A. Kovalčíková, Ľ. Medvecký, A. Naughton-Duszová, I. Vasková, J. Dusza
Abstract Advanced high-entropy (Hf-Ta-Zr-Nb-Ti)C ceramics were successfully fabricated by the combination of ball milling and a two-step sintering process at 2100 °C for 5, 10, and 20 minutes from commercially available powders. The microstructure characteristics and mechanical properties of the developed systems were investigated. The high-entropy ceramics exhibit: medium grain size from 8 μm to 11 μm, high compositional uniformity, and high relative density above 99.5 %. Vickers hardness for all systems decreased with increasing applied load, with the highest value HV1 = 22.0 GPa for the system sintered for 5 minutes, while the fracture toughness changed from 2.70 MPa.m1/2 to 3.50 MPa.m1/2. The highest four-point flexural strength of 284 MPa was measured for the system with the smallest grain size.
采用球磨和两步烧结工艺,在2100 °C温度下分别烧结5、10和20分钟,成功制备了先进的高熵(Hf-Ta-Zr-Nb-Ti)C陶瓷。研究了所制备体系的显微组织特征和力学性能。高熵陶瓷具有8 ~ 11 μm的中等晶粒尺寸、高均匀性和99.5%以上的相对密度等特点。各体系的维氏硬度均随外加载荷的增加而降低,烧结5min后的HV1为22.0 GPa,断裂韧性为2.70 MPa。m1/2到3.50 mpa。最小晶粒尺寸体系的四点抗弯强度最高为284 MPa。
{"title":"Effect of Sintering Time on Mechanical Properties of (Hf-Ta-Zr-Nb-Ti)C","authors":"Lenka Ďaková, M. Hrubovčáková, R. Sedlák, A. Kovalčíková, Ľ. Medvecký, A. Naughton-Duszová, I. Vasková, J. Dusza","doi":"10.2478/pmp-2021-0006","DOIUrl":"https://doi.org/10.2478/pmp-2021-0006","url":null,"abstract":"Abstract Advanced high-entropy (Hf-Ta-Zr-Nb-Ti)C ceramics were successfully fabricated by the combination of ball milling and a two-step sintering process at 2100 °C for 5, 10, and 20 minutes from commercially available powders. The microstructure characteristics and mechanical properties of the developed systems were investigated. The high-entropy ceramics exhibit: medium grain size from 8 μm to 11 μm, high compositional uniformity, and high relative density above 99.5 %. Vickers hardness for all systems decreased with increasing applied load, with the highest value HV1 = 22.0 GPa for the system sintered for 5 minutes, while the fracture toughness changed from 2.70 MPa.m1/2 to 3.50 MPa.m1/2. The highest four-point flexural strength of 284 MPa was measured for the system with the smallest grain size.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44413555","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Combined Effect of Phosphate and Polymer Coating on Cytotoxicity and Hemocompatibility of Iron Foams 磷酸盐和聚合物涂层对泡沫铁细胞毒性和血液相容性的联合影响
Q4 Materials Science Pub Date : 2021-12-01 DOI: 10.2478/pmp-2021-0005
R. Oriňaková, R. Gorejová, Martina Petráková, J. Macko, M. Kupková, M. Hrubovčáková, I. Maskalová
Abstract The use of resorbable metallic biomaterials for temporary implants has increased dramatically in the last decade. Degradable biomaterials are desirable in some specific pediatric, orthopedic, and cardiovascular applications, in which they may overcome the disadvantages of permanent devices. The three main biodegradable metals: Mg, Fe, and Zn, are intensively studied as temporary orthopedic implant materials. Among them, iron, and iron-based alloys, have received attention as promising materials for the temporary replacement of bones, especially for applications where strong mechanical support during the bone healing process is required. The addition of a low amount of phosphorus can improve the mechanical properties of such materials without the risk of retarding the corrosion rate or affecting cell proliferation. The main goal of this work was to study the combined effect of phosphating and polymer coating of open-cell iron foams on their cytotoxicity and hemocompatibility. Obtained results indicated the positive influence of the PEG coating layer and phosphorus addition on material cytocompatibility. Moreover, the combination of these procedures led to the inhibition of hemolysis, platelet adhesion, and thrombus formation.
摘要在过去十年中,可吸收金属生物材料在临时植入物中的应用急剧增加。可降解生物材料在一些特定的儿科、骨科和心血管应用中是可取的,在这些应用中,它们可以克服永久性装置的缺点。三种主要的可生物降解金属:镁、铁和锌,作为临时骨科植入材料进行了深入研究。其中,铁和铁基合金作为有前途的骨临时替代材料,特别是在骨愈合过程中需要强大机械支撑的应用中,受到了关注。添加少量的磷可以改善这种材料的机械性能,而没有延缓腐蚀速率或影响细胞增殖的风险。本工作的主要目的是研究开孔泡沫铁的磷化和聚合物涂层对其细胞毒性和血液相容性的联合影响。所得结果表明,PEG涂层和磷的添加对材料的细胞相容性有积极影响。此外,这些程序的结合导致溶血、血小板粘附和血栓形成的抑制。
{"title":"Combined Effect of Phosphate and Polymer Coating on Cytotoxicity and Hemocompatibility of Iron Foams","authors":"R. Oriňaková, R. Gorejová, Martina Petráková, J. Macko, M. Kupková, M. Hrubovčáková, I. Maskalová","doi":"10.2478/pmp-2021-0005","DOIUrl":"https://doi.org/10.2478/pmp-2021-0005","url":null,"abstract":"Abstract The use of resorbable metallic biomaterials for temporary implants has increased dramatically in the last decade. Degradable biomaterials are desirable in some specific pediatric, orthopedic, and cardiovascular applications, in which they may overcome the disadvantages of permanent devices. The three main biodegradable metals: Mg, Fe, and Zn, are intensively studied as temporary orthopedic implant materials. Among them, iron, and iron-based alloys, have received attention as promising materials for the temporary replacement of bones, especially for applications where strong mechanical support during the bone healing process is required. The addition of a low amount of phosphorus can improve the mechanical properties of such materials without the risk of retarding the corrosion rate or affecting cell proliferation. The main goal of this work was to study the combined effect of phosphating and polymer coating of open-cell iron foams on their cytotoxicity and hemocompatibility. Obtained results indicated the positive influence of the PEG coating layer and phosphorus addition on material cytocompatibility. Moreover, the combination of these procedures led to the inhibition of hemolysis, platelet adhesion, and thrombus formation.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41859663","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Announcements: Eva Dudrová – 80 years 公告:Eva Dudrová–80岁
Q4 Materials Science Pub Date : 2021-12-01 DOI: 10.2478/pmp-2021-0007
M. Kupková, P. Hvizdoš
{"title":"Announcements: Eva Dudrová – 80 years","authors":"M. Kupková, P. Hvizdoš","doi":"10.2478/pmp-2021-0007","DOIUrl":"https://doi.org/10.2478/pmp-2021-0007","url":null,"abstract":"","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2021-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47505724","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
Powder Metallurgy Progress
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1