The effect of different curing units on the degree of polymerization of different composite resins

O. Karatas, M. Yılmaz, Pınar Gul, O. Sagsoz, M. Yapar
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Abstract

Objective: The aim of this study was to investigate the degree of polymerization of composite resins cured with different light-curing units (LCUs). Materials and Methods: Three bulk-fill composite (Beautifil Bulk-Fill Giomer, Filtek Bulk-Fill, and X-Tra Fill) and a methacrylate-based composite (Filtek Z250) were used in this study. Thirty disc-shaped specimens, 4 mm thick, were prepared from each composite resin. Specimens were divided into three groups and polymerized with light-emitting diode (LED), Plasma arch curing unit (PAC), and quartz-tungsten halogen LCU. The bottom and top surface microhardness of the specimens stored in distilled water for 24 h at 37°C after polymerization was measured with a universal test device. The hardness ratio (HR) of specimens was calculated by the bottom surface microhardness/top surface microhardness formula. Data were analyzed by two-way ANOVA and Tukey's least significant difference post hoc tests (α = 0.05). Results: Statistically significant differences were detected between the mean HR values of the specimens polymerized with different LCUs (P < 0.05). The mean HR values of Beautifil Bulk-Fill Giomer specimens were found to be statistically significantly lower than other composites (P < 0.05). The mean HR values of the specimens polymerized with PAC LCU were found to be statistically significantly lower than other LCUs (P < 0.05). Conclusion: The degree of polymerization of the composite resin restoration may be affected by the structural properties of the resin and the type of LCU. The clinician may use alternative techniques, especially in deep cavities.
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不同固化单元对不同复合树脂聚合度的影响
目的:研究不同光固化单元(LCU)固化的复合树脂的聚合度。材料和方法:本研究使用了三种散装填充复合材料(Beautifil bulk-fill Giomer、Filtek bulk fill和X-Tra-fill)和一种基于甲基丙烯酸酯的复合材料(Filtek Z250)。由每种复合树脂制备了30个4mm厚的圆盘状试样。样品被分为三组,并与发光二极管(LED)、等离子弧固化单元(PAC)和石英-钨-卤素LCU聚合。使用通用测试装置测量聚合后在37°C的蒸馏水中储存24小时的试样的底部和顶部表面显微硬度。试样的硬度比(HR)由底表面显微硬度/顶表面显微硬度公式计算。采用双向方差分析和Tukey最小显著性差异事后检验(α=0.05)对数据进行分析。结果:用不同LCU聚合的样品的平均HR值之间存在统计学上的显著差异(P<0.05)。Beautifil Bulk-Fill Giomer样品的平均HR值被发现在统计学上显著低于其他复合材料(P<0.05)。PAC-LCU聚合的试件的平均HR值在统计学上显著低于其他LCU(P<0.05)。结论:复合树脂修复体的聚合程度可能受到树脂结构性能和LCU类型的影响。临床医生可以使用替代技术,尤其是在深腔中。
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