Degumming of Eri silk by Sapindus (soapnut) extract and optimisation by response surface methodology

IF 2 4区 工程技术 Q3 CHEMISTRY, APPLIED Coloration Technology Pub Date : 2023-02-20 DOI:10.1111/cote.12684
Harshal Patil, Krupali Surve, Ashok Athalye
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Abstract

The present investigation aims to develop a method for degumming Eri silk using Sapindus (soapnut) extract and optimise it using response surface methodology (RSM). The initial experiment was conducted with 10 g/L Sapindus extract for 60 min at a boil, and the initial experiments indicated effective degumming. Further degumming experiments were conducted using RSM to optimise the process parameters, with weight loss being the primary response. The results revealed an optimised recipe for degumming was 9 g/L Sapindus extract at 92°C for 30 min, and the desirability value for this optimised recipe is 0.376. Eri silk that has been alkali-degummed loses more weight than silk degummed with Sapindus extract and soap. Comparatively speaking, degumming with Sapindus extract has a lesser impact on tensile strength than degumming with alkaline and soap. The whiteness, yellowness, brightness, and absorbency values between Sapindus extract and conventional degumming do not significantly differ. Compared with soap and Sapindus extract degumming, alkaline degummed fabric exhibits higher dye uptake. After being degummed with soap and Sapindus extract instead of alkaline, the fabric felt softer. Overall, the results show that both degumming with Sapindus extract and traditional methods are equally effective.

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皂荚提取物对蚕丝的脱胶及响应面法优化
本研究旨在建立一种利用皂子提取物对蚕丝进行脱胶的方法,并利用响应面法(RSM)对其进行优化。初始实验采用10 g/L皂角提取物煮沸60 min,初始实验显示脱胶效果良好。使用RSM进行进一步的脱胶实验以优化工艺参数,以减重为主要响应。结果表明,皂荚脱胶的最佳配方为9 g/L皂荚提取物,温度为92℃,脱胶时间为30 min,理想值为0.376。用碱脱胶的蚕丝比用皂荚提取物和肥皂脱胶的蚕丝减轻了更多的重量。比较而言,皂角提取物脱胶对拉伸强度的影响小于碱脱胶和皂脱胶。白度、黄度、亮度、吸光度与常规脱胶无显著差异。碱性脱胶织物的染料吸收率高于皂液脱胶和皂液脱胶。用肥皂和皂荚提取物代替碱液脱胶后,织物感觉更柔软。综上所述,皂角提取物脱胶与传统方法脱胶效果相同。
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来源期刊
Coloration Technology
Coloration Technology 工程技术-材料科学:纺织
CiteScore
3.60
自引率
11.10%
发文量
67
审稿时长
4 months
期刊介绍: The primary mission of Coloration Technology is to promote innovation and fundamental understanding in the science and technology of coloured materials by providing a medium for communication of peer-reviewed research papers of the highest quality. It is internationally recognised as a vehicle for the publication of theoretical and technological papers on the subjects allied to all aspects of coloration. Regular sections in the journal include reviews, original research and reports, feature articles, short communications and book reviews.
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