EXTRACTION EXTRACTION AND CHARACTERIZATION OF PECTIN FROM LEMON LIME PEEL WASTE (Citrus amblycarpa)

Fiqi Estuning Nava Maulida, A. Alimuddin, Erwin Erwin
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Abstract

Research on the extraction and characterization of pectin from lemon lime peel waste (Citrus amblycarpa) has been done. The purpose of this research is to process lime waste into raw material of pectin source, to know pectin quality of extract obtained, and characterization pectin using FTIR spectrum. To obtain the results of research conducted several stages of research are pectin extraction, pectin precipitation, pectin washing, pectin drying and continued with the characterization of pectin which includes determination of moisture content, ash content, equivalent weight, methoxyl content, galakturonat level, esterification degree and spectrum analysis FTIR to determine the absorption of pectin functional groups obtained. The results showed that the yield% was 11.72%, the water content was 11.40%, the ash content was 1.34%, the weight of the equivalent was 871.5, the metoxyl content was 5.66, the galactonate level was 64.48 %, degree of esterification equal to 49,84% and FTIR analysis result which have conformity with standard pectin group that has OH, CH aliphatic, C = O, CH3 and CO group (secondary alcohol, carboxylic, ester, ether).
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从柠檬石灰渣中提取果胶及其性质研究
对柠檬酸橙皮渣中果胶的提取及性质进行了研究。本研究的目的是将石灰渣加工成果胶来源的原料,了解所得提取物的果胶质量,并利用红外光谱对果胶进行表征。为了获得研究结果,进行了几个阶段的研究,包括果胶提取、果胶沉淀、果胶洗涤、果胶干燥,并继续对果胶进行表征,包括测定水分含量、灰分含量、当量、甲氧基含量、半乳糖醛酸水平,酯化度和光谱分析FTIR测定果胶官能团的吸收得到。结果表明,产率为11.72%,水含量为11.40%,灰分为1.34%,当量重量为871.5,甲氧基含量为5.66,半乳糖酸盐含量为64.48%,酯化度为49,84%,FTIR分析结果符合OH,CH脂肪族,C=O的标准果胶基团,CH3和CO基团(仲醇、羧酸、酯、醚)。
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审稿时长
16 weeks
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