Magnetic and dielectric properties of 0.1 Bi2/3Cu3Ti4O12 -0.9 Bi3LaTi3O12 nanocomposite prepared by semi-wet route

Q3 Materials Science Current Nanomaterials Pub Date : 2022-08-20 DOI:10.2174/2405461507666220820121450
Pooja Gautam, A. Bharti, A. Tiwari, K. Mandal
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Abstract

A chemical formula of nanocomposite 0.1 Bi2/3Cu3Ti4O12 -0.9 Bi3LaTi3O12 (BCLT-19) was prepared by semiwet route using metal nitrate and solid TiO2. The phase formation of Bi2/3Cu3Ti4O12 (BCT) and Bi3LaTi3O12 (BLT) was confirmed by X-ray diffraction (XRD) study. Transmission electron microscope (TEM) analysis showed a nano particle of size 14 ± 5 nm on average for BCLT-19 composites. Scanning electron microscope (SEM) images exhibited a tubular, spherical and heterogeneous structure of grains. The root means square roughness, average roughness and maximum area peak height were explained by atomic force microscopy (AFM). Study of magnetic properties was determined as weak antiferromagnetic to ferromagnetic and in nature. The high dielectric constant (ε' = 3147 at 100Hz to 500 K) of BCLT-19 may be due to the existence of space charge polarization. In this manuscript have studies on the novel composite materials of BCLT-19 micro-structural properties. This is useful for future Random-access memory devices and dielectric materials,
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半湿法制备0.1Bi2/3Cu3Ti4O12-0.9Bi3LaTi3O12纳米复合材料的磁性和介电性能
以金属硝酸盐和固体TiO2为原料,通过半湿法合成了纳米复合材料0.1Bi2/3Cu3Ti4O12-0.9Bi3LaTi3O12(BCLT-19)。通过X射线衍射(XRD)研究证实了Bi2/3Cu3Ti4O12(BCT)和Bi3LaTi3O12(BLT)的相形成。透射电子显微镜(TEM)分析显示,BCLT-19复合材料的平均尺寸为14±5nm的纳米粒子。扫描电子显微镜(SEM)图像显示出管状、球形和非均匀的晶粒结构。用原子力显微镜(AFM)对其均方根粗糙度、平均粗糙度和最大面积峰高进行了解释。磁性能的研究被确定为弱反铁磁性到铁磁性以及在自然界中。BCLT-19的高介电常数(ε′=3147,在100Hz至500K下)可能是由于空间电荷极化的存在。本文对新型复合材料BCLT-19的微观结构性能进行了研究。这对于未来的随机存取存储器器件和介电材料是有用的,
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来源期刊
Current Nanomaterials
Current Nanomaterials Materials Science-Materials Science (miscellaneous)
CiteScore
1.60
自引率
0.00%
发文量
53
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