Growth inhibiting during ultra-high temperature sintering of injection moulded 17-4 PH stainless steel through the dispersion of ZrO2 particle as a thermal stabiliser

IF 1.9 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Powder Metallurgy Pub Date : 2022-05-31 DOI:10.1080/00325899.2022.2069076
Masoud Moradjoy, H. Khorsand
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Abstract

ABSTRACT The present work deals with the metal injection moulding and ultra-high temperature sintering of 17-4 PH powder. Purposefully, 5 mass% ZrO2 particles were dispersed by applying high shear stress during feedstock preparation. Uniformly distributed particles effectively hindered the powder boundary migration and limited their growth during ultra-high sintering temperatures. The achieved thermal stability provided a proper condition for reducing the final porosity to 3% and significantly improved the ultimate strength to 1070 MPa after sintering at 1380°C. Also, the ZrO2 particles acted as facilitators of sliding between solid powders and substantially reduced the required pressure for injecting to 700 Bar. Through introducing such a new approach in the field of powder injection moulding by ZrO2 particles, the amount of anisotropic shrinkage was reduced to 2%.
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通过分散ZrO2颗粒作为热稳定剂在注射成型17-4PH不锈钢的超高温烧结过程中抑制生长
本文研究了17-4PH粉末的金属注射成型和超高温烧结。有目的地,通过在原料制备过程中施加高剪切应力来分散5质量%的ZrO2颗粒。在超高烧结温度下,均匀分布的颗粒有效地阻碍了粉末边界的迁移并限制了它们的生长。所获得的热稳定性为将最终孔隙率降低至3%提供了合适的条件,并显著提高了极限强度至1070 在1380°C下烧结后的MPa。此外,ZrO2颗粒起到促进固体粉末之间滑动的作用,并显著降低了注射所需的压力至700巴。通过在ZrO2颗粒粉末注射成型领域引入这种新方法,各向异性收缩量减少到2%。
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来源期刊
Powder Metallurgy
Powder Metallurgy 工程技术-冶金工程
CiteScore
2.90
自引率
7.10%
发文量
30
审稿时长
3 months
期刊介绍: Powder Metallurgy is an international journal publishing peer-reviewed original research on the science and practice of powder metallurgy and particulate technology. Coverage includes metallic particulate materials, PM tool materials, hard materials, composites, and novel powder based materials.
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