Wear and Hardness Studies of Graphene Decorated with Graphene Quantum Dots (G-D-GQD) Embedded Epoxy Nano Composites

Q4 Materials Science Journal of Surface Science and Technology Pub Date : 2019-06-25 DOI:10.18311/JSST/2019/20103
Manuel George, A. Mohanty
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Abstract

The paper discusses about the wear and micro hardness behavior of Graphene Decorated with Graphene Quantum Dots (G-D-GQD) reinforced epoxy composites. The samples were prepared by open mold casting method by adding 0.25–1 wt. % (in an interval of 0.25%) of GDGQD and evaluated on a reciprocating wear tester configuration for wear and coefficient of friction properties. The micro-hardness testing of the G-D-GQD particles embedded epoxy composites has been performed and the hardness value results were compared with neat epoxy to find the improvement in hardness. Significant improvements in the hardness and wear resistance of the epoxy nanocomposites was obtained by the embedding of G-DGQD fillers, which is due to the efficient bonding of GDGQD filler with the epoxy matrix. Scanning Electron Microscope (SEM) images of the worn composites were analysed to get an insight into the morphology of the surfaces. Furthermore, the coefficient of friction of the composites got increased with the wt. % of fillers in the base material, but due to the superior bond strength and lesser agglomeration of the particles, the Vicker's hardness improved and the wear loss reduced. Hence the surface area coverage of G-D-GQDs got a significant role in the reduced wear loss and thereby coming to a threshold value. The study concludes by suggesting that 0.25 wt. % GDGQD/epoxy composites shown a least wear rate and increased hardness of 0.023% and 26%, respectively thereby suggesting application involving reduced wear rates.
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石墨烯量子点(G-D-GQD)嵌入环氧纳米复合材料修饰石墨烯的磨损和硬度研究
本文讨论了石墨烯量子点修饰石墨烯(G-D-GQD)增强环氧树脂复合材料的磨损和显微硬度行为。样品通过开模铸造法通过添加0.25–1 wt.%(间隔0.25%)的GDGQD制备,并在往复式磨损试验机配置上评估磨损和摩擦系数性能。对G-D-GQD颗粒嵌入环氧树脂复合材料进行了显微硬度测试,并将硬度值结果与纯环氧树脂进行了比较,以发现硬度的提高。通过嵌入G-DGQD填料,环氧树脂纳米复合材料的硬度和耐磨性得到了显著提高,这是由于GDGQD填料与环氧树脂基体的有效结合。分析了磨损复合材料的扫描电子显微镜(SEM)图像,以深入了解表面的形态。此外,随着基体材料中填料的重量百分比的增加,复合材料的摩擦系数增加,但由于其优异的粘结强度和较小的颗粒团聚,Vicker硬度提高,磨损损失降低。因此,G-D-GQDs的表面积覆盖率在减少磨损损失方面发挥了重要作用,从而达到阈值。该研究的结论是,0.25wt.%GDGQD/环氧树脂复合材料显示出最小的磨损率,硬度分别提高了0.023%和26%,从而表明应用涉及降低的磨损率。
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期刊介绍: The Indian Society for Surface Science and Technology is an organization for the cultivation, interaction and dissemination of knowledge in the field of surface science and technology. It also strives to promote Industry-Academia interaction
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