Towards innovative, successful and cost-efficient use of beam time

IF 16.4 1区 化学 Q1 CHEMISTRY, MULTIDISCIPLINARY Accounts of Chemical Research Pub Date : 2020-01-29 DOI:10.3233/jnr-200147
E. Lelièvre-Berna, P. Willendrup
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Abstract

This double issue presents some of the work accomplished by two Joint Research Activities (JRAs) of the project World class Science and Innovation with Neutrons in Europe 2020 (SINE2020) financed by the European Commission under the 8th Framework Programme. Within these two JRAs entitled E-tools for Instrumentation and Sample Environment, efforts have been made to explore the full potential of the large scale facilities and enable challenging experiments required by the neutron and muon user communities. In the following pages, we present new McStas components based on Monte-Carlo algorithms to optimise the signal to background ratio, a decisive factor for the success of many experiments. The first McStas bundle allows evaluating one of the major contributions to dose rate around neutron guides. Combined with the next article presenting the investigation of the neutron activation properties of the PE-B4C-concrete recently developed for the European Spallation Source (ESS), this will help facilities to optimise the siting of guides and instruments. The second presented McStas bundle calculates neutron pathways through materials surrounding samples which are generally the most difficult to screen. For the first time, textured materials are considered, taking elastic and inelastic scattering into account, including multiple scattering. The article is followed by a review of different materials for building novel pressure cells for inelastic scattering whose measurements have allowed to determine the effective phonon generalised density of states of these materials, a prerequisite for performing simulations. The next two articles focus on pressure devices. The first one presents the developments of gasket-anvil assemblies for the Paris–Edinburgh cell with 30% improved pressure performance giving a similar signal-to-background ratio. It also describes an improved Bridgman seal package which makes the low-temperature operation of the PE press significantly more reliable. The second article describes a new cell for the investigation of hydrogen storage materials at pressures up to 700 bar and temperatures up to 500°C. The following articles present a simple but very efficient technique for reducing the cool-down times of blue series furnaces by a factor 4 to 5, a comprehensive suite of sample environment equipment for efficient running of muon chemistry experiments over a wide range of conditions, and a portable single-sided NMR setup adapted to a small angle neutron scattering instrument for retrieving both structural and dynamical informations from a single experiment. This issue ends with an article demonstrating that rectangular beam cross-sections with a height over width ratio which mimic the ESS “pancake” moderator beams will lead to an improved homogeneity of the magnetic field integrals of spin echo instruments and an introduction to SECoP, the international Sample Environment Communication Protocol developed on close collaboration with the International Society for Sample Environment. Enjoy the reading!
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朝着创新、成功和经济有效地利用波束时间的方向发展
本期双刊介绍了欧盟委员会根据第八个框架计划资助的2020年欧洲中子世界级科学与创新项目(SINE2020)的两个联合研究活动(JRA)完成的一些工作。在这两个题为“仪器和样品环境电子工具”的联合研究报告中,已经努力探索大型设施的全部潜力,并实现中子和μ介子用户群体所需的具有挑战性的实验。在接下来的几页中,我们介绍了基于蒙特卡罗算法的新的McStas组件,以优化信号与背景比,这是许多实验成功的决定性因素。第一个McStas束允许评估中子引导周围剂量率的主要贡献之一。结合下一篇文章,介绍了最近为欧洲散裂源(ESS)开发的含PE-B4C混凝土的中子活化特性的研究,这将有助于设施优化导向器和仪器的选址。第二个给出的McStas束计算通过样本周围材料的中子路径,这些材料通常是最难筛选的。首次考虑了纹理材料,考虑了弹性和非弹性散射,包括多次散射。在这篇文章之后,我们回顾了用于构建新型非弹性散射压力电池的不同材料,这些材料的测量可以确定这些材料的有效声子广义态密度,这是进行模拟的先决条件。接下来的两篇文章主要讨论压力装置。第一篇介绍了巴黎-爱丁堡电池的垫圈-砧座组件的发展,其压力性能提高了30%,给出了类似的信号背景比。它还描述了一种改进的Bridgman密封封装,它使PE压机的低温操作更加可靠。第二篇文章描述了一种新的电池,用于研究压力高达700巴、温度高达500°C的储氢材料。以下文章介绍了一种将蓝色系列炉的冷却时间减少4到5倍的简单但非常有效的技术、一套用于在宽条件下有效运行μ介子化学实验的综合样品环境设备,以及适用于小角度中子散射仪器的便携式单侧NMR装置,用于从单个实验中检索结构和动力学信息。该问题以一篇文章结束,该文章证明了具有模仿ESS“煎饼”慢化剂光束的高宽比的矩形光束横截面将提高自旋回波仪器的磁场积分的均匀性,并介绍了SECoP,与国际样品环境学会密切合作制定的国际样品环境通信协议。享受阅读吧!
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Accounts of Chemical Research
Accounts of Chemical Research 化学-化学综合
CiteScore
31.40
自引率
1.10%
发文量
312
审稿时长
2 months
期刊介绍: Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.
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