The Study of Photocatalytic Behavior of Carbon-ZnS Nanocomposites Prepared with Microwave Co- precipitation Method

IF 1.4 Q4 NANOSCIENCE & NANOTECHNOLOGY Journal of Nanostructures Pub Date : 2020-07-01 DOI:10.22052/JNS.2020.03.001
Farnaz Maghazeii, D. Ghanbari, L. Lotfi
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引用次数: 3

Abstract

We prepared samples including nanoparticles of ZnS via co-precipitation method in room temperature and with microwave heating using water as a “green” solvent. The procedure was repeated with various natural surfactants. XRD and SEM analysis was performed to determine the nanostructural and morphologic characteristics of nanoparticles. The mean diameter less than 100 nm for ZnS particles showed that there was well-formed pure nanostructure. SEM analysis disclosed that temperature and type of surfactant will affect the nanostructures and so we can control the nanostructure and particle size with changing such parameters. With combining of pure Carbon and ZnS nanoparticles in various proportions, Carbon - ZnS nanocomposites was prepared using microwave heating. SEM and FT-IR analysis was performed on these nanocomposites to compare them with pure Carbon and ZnS nanoparticles. We also assessed the photocatalytic potential of prepared nanocomposites using acidic and neutral pH methyl orange and Congo red solutions under UV- IR radiation. This study confirms that these nanocomposites can be used as photo-catalysts for water refinery in home and industries.
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微波共沉淀法制备碳-锌纳米复合材料的光催化性能研究
我们在室温下通过共沉淀法和使用水作为“绿色”溶剂的微波加热制备了包括ZnS纳米颗粒的样品。用各种天然表面活性剂重复该程序。通过XRD和SEM分析,确定了纳米颗粒的纳米结构和形态特征。ZnS颗粒的平均直径小于100nm表明存在良好形成的纯纳米结构。SEM分析表明,表面活性剂的温度和类型会影响纳米结构,因此我们可以通过改变这些参数来控制纳米结构和颗粒尺寸。将纯碳和ZnS纳米颗粒按不同比例结合,利用微波加热制备了碳-ZnS纳米复合材料。对这些纳米复合材料进行SEM和FT-IR分析,将其与纯碳和ZnS纳米颗粒进行比较。我们还评估了使用酸性和中性pH甲基橙和刚果红溶液在紫外-红外辐射下制备的纳米复合材料的光催化潜力。本研究证实,这些纳米复合材料可作为光催化剂用于家庭和工业中的炼油厂。
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来源期刊
Journal of Nanostructures
Journal of Nanostructures NANOSCIENCE & NANOTECHNOLOGY-
CiteScore
2.60
自引率
0.00%
发文量
0
审稿时长
7 weeks
期刊介绍: Journal of Nanostructures is a medium for global academics to exchange and disseminate their knowledge as well as the latest discoveries and advances in the science and engineering of nanostructured materials. Topics covered in the journal include, but are not limited to the following: Nanosystems for solar cell, energy, catalytic and environmental applications Quantum dots, nanocrystalline materials, nanoparticles, nanocomposites Characterization of nanostructures and size dependent properties Fullerenes, carbon nanotubes and graphene Self-assembly and molecular organization Super hydrophobic surface and material Synthesis of nanostructured materials Nanobiotechnology and nanomedicine Functionalization of nanostructures Nanomagnetics Nanosensors.
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