Study of rapid thermal treatment on the microstructural evolution and surface characteristics of the electrodeposited modify Zn/TiO2 composite coatings on AISI 1015 steel

IF 1 4区 工程技术 Q4 ENGINEERING, MECHANICAL International Journal of Surface Science and Engineering Pub Date : 2018-09-16 DOI:10.1504/IJSURFSE.2018.10016053
O. Fayomi, A. A. Daniyan, L. E. Umoru, A. Popoola
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引用次数: 1

Abstract

In this study, the effect of systematic homogenising annealing heat treatment on the morphology and hardness property of modified Zn-TiO2 nano-composite coatings, coated via electrocodeposition process was investigated. The morphological characteristics of the composite coatings were characterised by scanning electron microscope (SEM) equipped with energy dispersive spectrometer (EDS) and the hardness examination was carried out using Dura-scan hardness tester. The result showed that the coatings systems were homogenised with refined microstructure after annealing at 250°C and 500°C. Three different inter-metallic structures; zeta, delta and gamma phase were observed after systematic homogenising annealing at 500°C. The hardness performance of the nano-composite coatings was better after the annealing at 250°C for five hours and showed outstanding improvement after systematically annealed at 500°C.
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快速热处理对aisi1015钢电沉积改性Zn/TiO2复合镀层组织演变及表面特征的研究
在本研究中,研究了系统均质退火热处理对电共沉积改性Zn-TiO2纳米复合涂层形貌和硬度的影响。采用扫描电镜(SEM)和能谱仪(EDS)对复合涂层的形貌特征进行了表征,并用Dura-scan硬度计对复合涂层进行了硬度测试。结果表明,在250℃和500℃退火后,涂层体系均质化,组织细化。三种不同的金属间结构;在500℃系统均质退火后观察到zeta, delta和gamma相。在250℃退火5 h后,纳米复合涂层的硬度性能较好,在500℃系统退火后,涂层的硬度有明显提高。
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来源期刊
CiteScore
1.60
自引率
25.00%
发文量
21
审稿时长
>12 weeks
期刊介绍: IJSurfSE publishes refereed quality papers in the broad field of surface science and engineering including tribology, but with a special emphasis on the research and development in friction, wear, coatings and surface modification processes such as surface treatment, cladding, machining, polishing and grinding, across multiple scales from nanoscopic to macroscopic dimensions. High-integrity and high-performance surfaces of components have become a central research area in the professional community whose aim is to develop highly reliable ultra-precision devices.
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