Nanoparticles Embedded In2O3 Microspheres for Selective and Quantitative Detection of NO2 Gas

IF 0.9 4区 材料科学 Science of Advanced Materials Pub Date : 2023-05-01 DOI:10.1166/sam.2023.4395
Sufaid Shah, S. Hussain, A. Shaheen, Guiwu Liu, M. Hashem, Majed M. Alsarani, M. S. Akhtar, You Tianyan, G. Qiao, Hassanein Fouad
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引用次数: 2

Abstract

Harmful consequences on human health have been caused by the rapidly rising levels of environmentally hazardous gases. It is necessary to detect these polluting gases using a variety of methods. Nanoparticles engraved spherical-shaped indium oxide structures are synthesized via a simple one-step solvothermal method. The synthesized products were successfully characterized using XRD, SEM, EDS, TEM and XPS analysis. Nanoparticle embedded In2O3 microspheres are prepared for selective, quantitative and low concentration (1–10 ppm) of NO2 gas detection at operating temperature of 75 °C–250 °C. A high sensing response of 29 is observed at 10 ppm with sharp response and recovery times of 44 s and 56 s at 200 °C, respectively. The superior performances towards NO2 gas is attributed to the presence of plenty of junctions between nanoparticles-microspheres surfaces and high surface area for gas molecules interactions. The fabricated sensors are promised and potential applicants in the environmental pollution detection devices on industrial scale.
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纳米In2O3微球选择性定量检测NO2气体
对环境有害气体含量的迅速上升对人类健康造成了有害后果。有必要使用各种方法来检测这些污染气体。采用简单的一步溶剂热法合成了球形氧化铟纳米颗粒。通过XRD、SEM、EDS、TEM和XPS等手段对合成产物进行了表征。在75℃~ 250℃的工作温度下,制备了纳米颗粒包埋In2O3微球,用于NO2气体的选择性、定量和低浓度(1 ~ 10ppm)检测。在10 ppm条件下观察到29的高传感响应,在200°C下分别为44 s和56 s的快速响应和恢复时间。纳米颗粒-微球表面之间存在大量的连接,并且气体分子相互作用的表面积很大,这是纳米颗粒对二氧化氮气体具有优异性能的原因。该传感器在工业环境污染检测设备中具有广阔的应用前景。
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来源期刊
Science of Advanced Materials
Science of Advanced Materials NANOSCIENCE & NANOTECHNOLOGY-MATERIALS SCIENCE, MULTIDISCIPLINARY
自引率
11.10%
发文量
98
审稿时长
4.4 months
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