Barium M-Hexaferrite BaFe12O19 Based on Magnetic Properties and Microwafe Absorption

Noer Af’idah, Oktaffi Arinna Manasikan, Andri Wahyu Wijayadi
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Abstract

Barium M-hexaferite is a material which has the potential to be developed as a magnetic material which is needed in various fields of application. Various methods have been used to produce this material, but in general these methods require heating at relatively high temperatures. This research was conducted to characterize the magnetic properties and microwave absorption of barium M-hexaferrite which was synthesized using the coprecipitation method by sintering at low temperatures. Synthesis of barium M-hexaferite was carried out using BaCO3, FeCl3. 6H2O, HCl, NH4OH. The results of the coprecipitation were dried using a light bulb at a temperature of 850C, then sintered at a 3000C with variations in holding times of 1 hour, 3 hours and 5 hours. The magnetic properties of the synthesized materials were tested using VSM, while the properties of microwave absorption were characterized using VNA. From the VSM test results, it can be determined that the highest remanence magnetization and coercivity values were found in the samples sintered at 3000C for 3 hours, namely Mr 0.103 emu/gram and Hc 0.058 Tesla. Meanwhile, from testing the absorption properties of the material for microwaves using VNA, it was found that the largest reflection loss value was found in the sample which was calcined for 3 hours, which was 52.4 dB or equivalent to an absorption of 99% at a frequency of 11 GHz. From the research it was found that barium M-hexaferite as a result of coprecipitation can be developed into a good microwave absorbent material.
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基于磁性和微波吸收的m -六铁体钡BaFe12O19
六价钡是一种有潜力发展成为各种应用领域所需的磁性材料的材料。已经使用了各种方法来生产这种材料,但通常这些方法需要在相对较高的温度下加热。本研究采用共沉淀法在低温下烧结合成了M-六铁氧体钡,对其磁性能和微波吸收进行了表征。使用BaCO3、FeCl3进行了M-六亚硫酸钡的合成。6H2O、HCl、NH4OH。使用灯泡在850℃的温度下干燥共沉淀的结果,然后在3000℃下烧结,保持时间变化为1小时、3小时和5小时。用VSM测试了合成材料的磁性能,用VNA表征了微波吸收性能。从VSM测试结果可以确定,在3000℃烧结3小时的样品中发现了最高的剩磁磁化强度和矫顽力值,即Mr 0.103 emu/g和Hc 0.058 Tesla。同时,通过使用VNA测试材料对微波的吸收特性,发现在煅烧3小时的样品中发现最大的反射损耗值,其为52.4dB或相当于在11GHz的频率下99%的吸收。通过研究发现,M-六亚硫酸钡作为共沉淀的结果可以发展成为一种良好的微波吸收材料。
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发文量
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审稿时长
24 weeks
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