Effect of solution treatment on microstructure and properties of 00Cr32Ni7Mo3.5N

IF 1.9 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Powder Metallurgy Pub Date : 2021-12-15 DOI:10.1080/00325899.2021.2014656
Yang Zhao, Jian-hao Chen, Meihuan Qi, S. Ren, X. Qu
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Abstract

ABSTRACT 00Cr32Ni7Mo3.5N parts were prepared by hot isostatic pressing (HIP) and forging process in this study. The effect of solution heat treatment on microstructure, mechanical properties and pitting resistance were investigated. Under solution treating at 1100°C, the phase constitution in HIP parts can be adjusted to comprise approximately 50% austenite (γ) and 50% ferrite (δ) phases with equiaxed structure, and this post-processing can meanwhile help to dissolve precipitated brittle σ phase. In comparison, the banded dual-phase structures in forged counterparts cannot be removed even after annealing at 1200°C. The desired phase proportion after solution treatment plus the equiaxed grains impart superior comprehensive performance to HIP parts with the tensile strength of 886 MPa, elongation of 48.0%, impact energy of 83 J, and pitting potential of 0.9659 V in neutral 3.5 wt-% NaCl solution. Based on this work, HIP seems to be a promising method to fabricate near-net-shape 00Cr32Ni7Mo3.5N parts. Highlights SAF3207 were prepared by HIP and was compared with its forging parts. HIP samples show equiaxed structure, while forgings are banded dual phase structures. Phase constitution can be adjusted to be approximately 50% austenite and 50% ferrite. The brittle σ phase can be completely removed after solution treatment. HIP seems a promising method to fabricate SAF3207 with high performance. GRAPHICAL ABSTRACT
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固溶处理对00Cr32Ni7Mo3.5N合金组织和性能的影响
本文采用热等静压和锻造工艺制备了00Cr32Ni7Mo3.5N零件。研究了固溶热处理对组织、力学性能和耐点蚀性能的影响。在1100°C的固溶处理下,HIP零件中的相组成可以调整为约50%的奥氏体(γ)和50%的铁素体(δ)相,具有等轴结构,这种后处理同时可以帮助溶解沉淀的脆性σ相。相比之下,即使在1200°C下退火,锻造对应物中的带状双相结构也无法去除。固溶处理后所需的相比例加上等轴晶粒使HIP零件具有优异的综合性能,抗拉强度为886 MPa,伸长率48.0%,冲击能83 J、 点蚀电位为0.9659 V在中性3.5 wt-%NaCl溶液。基于这项工作,HIP似乎是一种很有前途的制造近净形状00Cr32Ni7Mo3.5N零件的方法。亮点SAF3207由HIP制备,并与其锻件进行了比较。HIP试样为等轴组织,锻件为带状双相组织。可以将相组成调整为大约50%的奥氏体和50%的铁素体。经过固溶处理后,脆性σ相可以完全去除。HIP是制备高性能SAF3207的一种很有前途的方法。图形摘要
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来源期刊
Powder Metallurgy
Powder Metallurgy 工程技术-冶金工程
CiteScore
2.90
自引率
7.10%
发文量
30
审稿时长
3 months
期刊介绍: Powder Metallurgy is an international journal publishing peer-reviewed original research on the science and practice of powder metallurgy and particulate technology. Coverage includes metallic particulate materials, PM tool materials, hard materials, composites, and novel powder based materials.
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