Microstructural Evolution and Mechanical Properties According to Aging Conditions of Ti-5Mo-2Fe Alloy

IF 1.1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Korean Journal of Metals and Materials Pub Date : 2023-08-05 DOI:10.3365/kjmm.2023.61.8.545
Hong-Min Kim, Se-Yeong Park, Dong-Geun Lee
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Abstract

Beta-type titanium alloys have a low elastic modulus, excellent cold workability, and are widely used as implant materials. High strength is possible by forming a precipitation in the β-matrix via solution treatment and aging treatment. However, beta titanium alloys require a large amount of beta-stabilizing elements (Fe, Nb, Mo, Ta, etc), and these expensive beta stabilizing elements increase the manufacturing cost of these alloys. In this study, Ti-5Mo-2Fe metastable beta-titanium alloy was designed by adding Mo and Fe, which were relatively inexpensive and had excellent biocompatibility among beta-stabilizing elements, and an ingot was manufactured by vacuum arc remelting. Solution treatment was maintained at 850oC for a holding time of 1 hour, followed by furnace cooling. Aging treatments were conducted in a range of temperature 350~500oC and holding time 2 h~48 h. The microstructure behaviors and mechanical properties were analyzed according to these aging treatment conditions. Isothermal ω phases were precipitated by aging treatment, and hardness and yield strength were found to be significantly higher for conditions of 400oC, 8h. As holding time and temperature increased, these phases transformed into secondary alpha phases and the hardness and yield strength decreased due to this microstructural evolution.
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Ti-5Mo-2Fe合金时效条件下的组织演变和力学性能
β型钛合金具有弹性模量低、冷加工性好等优点,被广泛用作植入材料。通过固溶处理和时效处理在β-基体中形成析出物,可获得较高的强度。然而,β钛合金需要大量的β稳定元素(Fe、Nb、Mo、Ta等),这些昂贵的β稳定元素增加了这些合金的制造成本。本研究通过添加相对便宜且稳定元素间具有良好生物相容性的Mo和Fe,设计了Ti-5Mo-2Fe亚稳态β钛合金,并采用真空电弧重熔法制备了铸锭。固溶处理在850℃下保持1小时,然后进行炉膛冷却。在温度350~500℃,保温时间2 h~48 h的条件下进行时效处理,并根据时效条件对合金的组织行为和力学性能进行分析。时效处理可析出等温ω相,在400oC, 8h条件下硬度和屈服强度显著提高。随着保温时间的延长和保温温度的升高,这些相转变为次生α相,硬度和屈服强度下降。
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来源期刊
Korean Journal of Metals and Materials
Korean Journal of Metals and Materials MATERIALS SCIENCE, MULTIDISCIPLINARY-METALLURGY & METALLURGICAL ENGINEERING
CiteScore
1.80
自引率
58.30%
发文量
100
审稿时长
4-8 weeks
期刊介绍: The Korean Journal of Metals and Materials is a representative Korean-language journal of the Korean Institute of Metals and Materials (KIM); it publishes domestic and foreign academic papers related to metals and materials, in abroad range of fields from metals and materials to nano-materials, biomaterials, functional materials, energy materials, and new materials, and its official ISO designation is Korean J. Met. Mater.
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