Ayben Kilic-Pekgözlü, E. Ceylan, A. Gençer, R. Kurt
{"title":"Optimization for Green Path in Wood Extractives by Taguchi Analysis","authors":"Ayben Kilic-Pekgözlü, E. Ceylan, A. Gençer, R. Kurt","doi":"10.5552/drvind.2022.2137","DOIUrl":null,"url":null,"abstract":"Extractive composition of Pinus pinaster (Maritime pine) wood was studied with choline chloride based deep eutectic solvents (DES). Two different eutectic mixtures (ChCl: Et-Gly; ChCl:Urea 1:2 molar ratio), two different extraction methods (hot water bath, ultrasound assisted extraction), and temperature (40 – 60 °C), time (30 – 60 min.) and solid:liquid ratio (1:10 – 1:20 g/mL) parameters were applied. For the optimization of operation conditions, Taguchi analysis was performed. Resin acids formed the chemical composition of Pinus pinaster (Maritime pine) wood. Dehydroabietic acid, abietic acid and isopimaric acid were found to be the major compounds. The impact of parameters on the performance of the system was determined as follows: DES type > solid:liquid ratio > extraction method > temperature > time. So, for the extraction of lipophilic compounds in Maritime pine wood, the optimum conditions were determined as hot water bath extraction at 60 °C with ethylene glycol and 1:10 solid liquid ratio for 60 min.","PeriodicalId":11427,"journal":{"name":"Drvna Industrija","volume":null,"pages":null},"PeriodicalIF":0.7000,"publicationDate":"2022-11-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Drvna Industrija","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.5552/drvind.2022.2137","RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, PAPER & WOOD","Score":null,"Total":0}
引用次数: 0
Abstract
Extractive composition of Pinus pinaster (Maritime pine) wood was studied with choline chloride based deep eutectic solvents (DES). Two different eutectic mixtures (ChCl: Et-Gly; ChCl:Urea 1:2 molar ratio), two different extraction methods (hot water bath, ultrasound assisted extraction), and temperature (40 – 60 °C), time (30 – 60 min.) and solid:liquid ratio (1:10 – 1:20 g/mL) parameters were applied. For the optimization of operation conditions, Taguchi analysis was performed. Resin acids formed the chemical composition of Pinus pinaster (Maritime pine) wood. Dehydroabietic acid, abietic acid and isopimaric acid were found to be the major compounds. The impact of parameters on the performance of the system was determined as follows: DES type > solid:liquid ratio > extraction method > temperature > time. So, for the extraction of lipophilic compounds in Maritime pine wood, the optimum conditions were determined as hot water bath extraction at 60 °C with ethylene glycol and 1:10 solid liquid ratio for 60 min.
期刊介绍：
"Drvna industrija" ("Wood Industry") journal publishes original scientific and review papers, short notes, professional papers, conference papers, reports, professional information, bibliographical and survey articles and general notes relating to the forestry exploitation, biology, chemistry, physics and technology of wood, pulp and paper and wood components, including production, management and marketing aspects in the woodworking industry.
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