Synthesis and Evaluation of Strengthened Copper with 3 wt. % TiC and/ or Al2O3 Prepared By SPS Technique

Fadel S. Hamid, A. Elsayed, O. Elkady, A. El-Nikhaily, A. Essa
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Abstract

Cu-(TiC/Al2O3) nanocomposite was synthesized successfully using the powder metallurgy route. The constituents are first ball-milled and then sintered using the spark plasma sintering technique. The tribological and physical properties are investigated. The homogeneity and of ceramics distribution were also evaluated using SEM and XRD. Results showed that TiC and Al2O3 nanoparticles were homogeneously distributed all over the Cu matrix. Copper reinforced with 3 wt.% Al2O3 and hybrid (3 wt. % TiC and Al2O3) had the lowest relative density (95 %). The hybrid (3 wt. % TiC and Al2O3) sample had a higher wear rate value (1.7 * 10-3) at 25 N load, while the sample reinforced with 3 wt.% TiC had the lowest value (0.5 * 10-3) at 25 N load. Cu-Al2O3 exhibited a higher hardness value (149 HV). The highest electrical and thermal conductivities are recorded for the Cu -TiC that were (20.76 MS/m) and (149.03 W/m. k) respectively.
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SPS技术制备的3wt.%TiC和/或Al2O3增强铜的合成与评价
采用粉末冶金方法成功合成了Cu-(TiC/Al2O3)纳米复合材料。成分首先进行球磨,然后使用火花等离子体烧结技术进行烧结。对其摩擦学性能和物理性能进行了研究。利用SEM和XRD对陶瓷的均匀性和分布进行了评价。结果表明,TiC和Al2O3纳米颗粒均匀分布在Cu基体上。用3wt.%Al2O3和杂化物(3wt.%TiC和Al2O3)增强的铜具有最低的相对密度(95%)。混合(3wt.%TiC和Al2O3)样品在25N载荷下具有较高的磨损率值(1.7*10-3),而用3wt.%TiC增强的样品在25n载荷下具有最低值(0.5*10-3)。Cu-Al2O3表现出较高的硬度值(149HV)。Cu-TiC的最高电导率和热导率分别为(20.76 MS/m)和(149.03 W/m.k)。
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