Surface Enhancement of Additively Manufactured Bone Plate Through Hybrid-Electrochemical Magnetorheological Finishing Process.

IF 4.7 Q2 MATERIALS SCIENCE, BIOMATERIALS ACS Applied Bio Materials Pub Date : 2024-06-18 eCollection Date: 2024-06-01 DOI:10.1089/3dp.2023.0028
Atul Singh Rajput, Sajan Kapil, Manas Das
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Abstract

Additive manufacturing or 3D printing provides the benefits of individualizing the implant per patient requirements. However, the poor surface quality of additively manufactured biomaterial is a major limitation. Hence, hybrid-electrochemical magnetorheological (H-ECMR) polishing is developed to improve the surface quality of fabricated parts. H-ECMR finishing is an advanced surface polishing operation that avails the synergic action of mechanical abrasion and the electrochemical reaction to enhance the surface quality of the workpiece without hampering its surface topography. Furthermore, the developed H-ECMR finishing process reduces the finishing time and produces a uniform surface quality compared with the conventional magnetorheological (MR) finishing process. However, the surface finishing of the parts having a hole-of-pocket feature through the H-ECMR finishing process is a major challenge as MR fluid gets trapped inside those holes or pockets. A feature-based hybrid H-ECMR finishing process is developed to resolve the issue. In this case, paraffin wax is applied to the holes and pockets before the H-ECMR process occurs. In the present work, bone plates are fabricated through selective laser melting, and their surface quality is further enhanced through the H-ECMR finishing process. Bone plates are necessary to provide mechanical stability during bone fracture healing by adapting to the chemical environment. The final Ra value of 21.37 nm is attained from 9.36 μm through H-ECMR finishing. Pin-on-disk study is carried out on the biomaterial to analyze its wear resistance. The surface topography of the workpiece is analyzed through scanning electron microscopy before and after finishing, and it was observed that a uniform surface is achieved after polishing. Apart from the average surface roughness (Ra ), other roughness parameters such as skewness (R sk) and kurtosis (R ku) are analyzed to study the attribute of the surface irregularities.

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电化学-磁流变复合抛光工艺对增材骨板的表面增强
增材制造或三维打印技术的优点是可以根据患者的要求个性化植入假体。然而,增材制造生物材料的表面质量差是一个主要限制因素。因此,混合电化学磁流变(H-ECMR)抛光技术应运而生,以改善制造部件的表面质量。H-ECMR 抛光是一种先进的表面抛光操作,它利用机械磨损和电化学反应的协同作用,在不影响工件表面形貌的情况下提高工件的表面质量。此外,与传统的磁流变(MR)精加工工艺相比,所开发的 H-ECMR 精加工工艺缩短了精加工时间,并能获得均匀的表面质量。然而,通过 H-ECMR 光饰工艺对具有孔洞特征的零件进行表面光饰是一项重大挑战,因为磁流变液会滞留在这些孔洞或凹槽内。为了解决这个问题,我们开发了一种基于特征的混合 H-ECMR 光饰工艺。在这种情况下,在进行 H-ECMR 处理之前,会在孔和凹陷处涂上石蜡。在目前的工作中,骨板是通过选择性激光熔化制造的,并通过 H-ECMR 精加工工艺进一步提高了其表面质量。骨板通过适应化学环境,在骨折愈合过程中提供机械稳定性。通过 H-ECMR 精加工,Ra 值从 9.36 μm 最终达到 21.37 nm。对生物材料进行了针盘研究,以分析其耐磨性。通过扫描电子显微镜分析了精加工前后工件的表面形貌。除了平均表面粗糙度(Ra)外,还分析了其他粗糙度参数,如偏度(R sk)和峰度(R ku),以研究表面不规则的属性。
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来源期刊
ACS Applied Bio Materials
ACS Applied Bio Materials Chemistry-Chemistry (all)
CiteScore
9.40
自引率
2.10%
发文量
464
期刊介绍: ACS Applied Bio Materials is an interdisciplinary journal publishing original research covering all aspects of biomaterials and biointerfaces including and beyond the traditional biosensing, biomedical and therapeutic applications. The journal is devoted to reports of new and original experimental and theoretical research of an applied nature that integrates knowledge in the areas of materials, engineering, physics, bioscience, and chemistry into important bio applications. The journal is specifically interested in work that addresses the relationship between structure and function and assesses the stability and degradation of materials under relevant environmental and biological conditions.
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