Microscopic study of zinc nanoparticles synthesised using thermosetting polymer

Q3 Immunology and Microbiology Applied Microscopy Pub Date : 2019-12-31 DOI:10.1186/s42649-019-0018-0
Giriraj Tailor, Jyoti Chaudhay, Deepshikha Verma, Bhupendra Kr. Sarma
{"title":"Microscopic study of zinc nanoparticles synthesised using thermosetting polymer","authors":"Giriraj Tailor,&nbsp;Jyoti Chaudhay,&nbsp;Deepshikha Verma,&nbsp;Bhupendra Kr. Sarma","doi":"10.1186/s42649-019-0018-0","DOIUrl":null,"url":null,"abstract":"<p>The present study reports the novel synthesis of Zinc nanoparticles (Zn NPs) by thermal decomposition method and its characterisation by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and X-ray Diffraction Measurements (XRD). Synthesis of Zn NPs was achieved by using thermosetting polymer and zinc salts as precursor. Zn NPs were obtained on calcination at 850?°C for 30?min. SEM study reveals that synthesized nanoparticles are spherical in shape. XRD analysis shows that the Zn NPs formed are low crystalline in nature.</p>","PeriodicalId":470,"journal":{"name":"Applied Microscopy","volume":"49 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-12-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1186/s42649-019-0018-0","citationCount":"7","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Applied Microscopy","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1186/s42649-019-0018-0","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Immunology and Microbiology","Score":null,"Total":0}
引用次数: 7

Abstract

The present study reports the novel synthesis of Zinc nanoparticles (Zn NPs) by thermal decomposition method and its characterisation by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and X-ray Diffraction Measurements (XRD). Synthesis of Zn NPs was achieved by using thermosetting polymer and zinc salts as precursor. Zn NPs were obtained on calcination at 850?°C for 30?min. SEM study reveals that synthesized nanoparticles are spherical in shape. XRD analysis shows that the Zn NPs formed are low crystalline in nature.

Abstract Image

查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
热固性聚合物合成锌纳米颗粒的显微研究
本文报道了用热分解法合成锌纳米颗粒(Zn NPs)的新方法,并通过扫描电镜(SEM)、透射电镜(TEM)和x射线衍射仪(XRD)对其进行了表征。以热固性聚合物和锌盐为前驱体,合成了锌纳米粒子。在850℃下煅烧得到Zn NPs。°C 30min。SEM研究表明,合成的纳米颗粒呈球形。XRD分析表明,形成的Zn NPs具有低晶性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
Applied Microscopy
Applied Microscopy Immunology and Microbiology-Applied Microbiology and Biotechnology
CiteScore
3.40
自引率
0.00%
发文量
10
审稿时长
10 weeks
期刊介绍: Applied Microscopy is a peer-reviewed journal sponsored by the Korean Society of Microscopy. The journal covers all the interdisciplinary fields of technological developments in new microscopy methods and instrumentation and their applications to biological or materials science for determining structure and chemistry. ISSN: 22875123, 22874445.
期刊最新文献
Material analysis on semi-permanent makeup needles Analytical microscopy techniques using coaxial and oblique illuminations to detect thin glass particulates generated from glass vials for parenteral drug products Correction: Microstructural, mechanical, and electrochemical analysis of carbon doped AISI carbon steels In situ observation of catalyst nanoparticle sintering resistance on oxide supports via gas phase transmission electron microscopy Research reviews on myosin head interactions with F-actin
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1