Optical and Morphological Properties of ZnO and TiO2 Derived Nanostructures Synthesized via a Microwave-Assisted Hydrothermal Method

IF 0.5 Q4 ENERGY & FUELS Advances in Energy Research Pub Date : 2012-02-29 DOI:10.1155/2012/189069
N. Moloto, S. Mpelane, L. Sikhwivhilu, S. Ray
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引用次数: 23

Abstract

A microwave-assisted hydrothermal method was used to synthesize ZnO and TiO2 nanostructures. The experimental results show that the method resulted in crystalline monodispersed ZnO nanorods that have pointed tips with hexagonal crystal phase. TiO2 nanotubes were also formed with minimum bundles. The mechanism for the formation of the tubes was validated by HRTEM results. The optical properties of both ZnO and TiO2 nanostructures showed characteristics of strong quantum confinement regime. The photoluminescence spectrum of TiO2 nanotubes shows good improvement from previously reported data.
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微波辅助水热法合成ZnO和TiO2纳米结构的光学和形态性质
采用微波辅助水热法制备了ZnO和TiO2纳米结构。实验结果表明,该方法制备的ZnO纳米棒具有尖端尖的六方晶相。形成的TiO2纳米管束也最小。HRTEM结果验证了管状结构的形成机理。ZnO和TiO2纳米结构的光学性质均表现出强量子约束体系的特征。TiO2纳米管的光致发光光谱较先前报道的数据有明显改善。
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Advances in Energy Research
Advances in Energy Research ENERGY & FUELS-
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