AN ACCESSIBLE GLOVE BOX PROJECT FOR PROCEDURES THAT REQUIRE INERT CONDITIONS

IF 0.5 4区 化学 Q4 CHEMISTRY, MULTIDISCIPLINARY Quimica Nova Pub Date : 2023-03-03 DOI:10.21577/0100-4042.20170966
Pedro Pereira, Jean de Andrade, Pedro Maia, G. Malpass
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Abstract

An inert atmosphere is, in some cases, important for the performing of experiments where substances are toxic and/or sensitive to oxygen. However, the high cost and accessibility of an equipment to work under these conditions, results in the fact that most laboratories do not have this kind of equipment. In this paper, we present a simple and efficient project to build a cheap glove box for processes that require an inert atmosphere. The proposed glove box is made using medium density fiberboard (MDF), an acrylic lid, hinges, air valves, PVC gloves and other materials that can be found easily in local stores or on the internet. Tests to verify the quality of the nitrogen atmosphere were performed using the lighter test and niobium pentachloride (NbCl5), which is a moisture/oxygen sensitive material. The results demonstrated that the equipment is able to maintain an inert atmosphere for several hours, does not permit lighter to function and maintains the NbCl5 stable.
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一个可访问的手套箱项目,用于需要惰性条件的程序
在某些情况下,惰性气氛对于进行有毒物质和/或对氧敏感的实验是很重要的。然而,在这些条件下工作的设备的高成本和可及性导致大多数实验室没有这种设备。在本文中,我们提出了一个简单而有效的项目,为需要惰性气氛的过程建立一个廉价的手套箱。设计中的手套箱由中密度纤维板(MDF)、丙烯酸盖、铰链、空气阀、PVC手套和其他在当地商店或互联网上很容易找到的材料制成。验证氮气气氛质量的测试使用了打火机测试和五氯化铌(NbCl5),这是一种对水分/氧气敏感的材料。结果表明,该设备能够保持几个小时的惰性气氛,不允许打火机工作,并保持NbCl5的稳定。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Quimica Nova
Quimica Nova 化学-化学综合
CiteScore
1.60
自引率
12.50%
发文量
72
审稿时长
2-4 weeks
期刊介绍: Química Nova publishes in portuguese, spanish and english, original research articles, revisions, technical notes and articles about education in chemistry. All the manuscripts submitted to QN are evaluated by, at least, two reviewers (from Brazil and abroad) of recognized expertise in the field of chemistry involved in the manuscript. The Editorial Council can be eventually asked to review manuscripts. Editors are responsible for the final edition of QN.
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